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MassMS-NW-8936 3-amino-alpha-methylbenzyl alcohol C8H11NO (Mass of molecular ion: 137)
Source Temperature: 260 °C Sample Temperature: 150 °C Reservoir, 75 eV
18.0 1.7 27.0 1.5 28.0 2.4 38.0 1.1 39.0 6.7 40.0 1.2 41.0 4.0 42.0 1.6 43.0 11.0 45.0 2.0 46.5 1.0 50.0 1.1 51.0 3.3 52.0 2.3 53.0 1.7 54.0 1.6 55.0 1.5 58.5 1.3 61.0 4.7 63.0 2.8 64.0 1.8 65.0 12.8 66.0 7.3 67.0 3.9 68.0 1.0 69.0 1.0 71.0 3.3 76.0 1.1 77.0 24.0 78.0 2.8 79.0 1.0 80.0 1.0 81.0 2.2 82.0 1.2 91.0 5.2 92.0 8.0 93.0 13.1 94.0 100.0 95.0 8.9 103.0 1.0 105.0 1.4 106.0 1.7 117.0 1.3 118.0 4.2 119.0 4.0 120.0 6.6 121.0 2.7 122.0 28.5 123.0 3.0 136.0 2.1 137.0 57.7 138.0 5.9
90 MHz in CDCl3
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1H NMR 89.56 MHz C8 H11 N O 0.035 g : 0.5 ml CDCl3 3-amino-alpha-methylbenzyl alcohol 
Assign. Shift(ppm)
A 7.090 B 6.70 C 6.65 D 6.55 E 4.727 F 3.3 G 1.419
Hz ppm Int.644.06 7.192 73 643.13 7.181 67 636.56 7.108 149 635.81 7.100 181 629.00 7.024 137 628.31 7.016 148 606.06 6.768 86 604.44 6.749 163 603.88 6.743 131 603.31 6.737 135 602.81 6.731 116 597.06 6.667 257 596.63 6.662 250 595.44 6.649 262 594.25 6.636 191 593.38 6.626 140 592.56 6.617 95 591.69 6.607 181 590.56 6.595 154 589.31 6.581 97 588.19 6.568 78 584.06 6.522 109 582.75 6.507 99 581.88 6.498 80 580.50 6.482 67 427.13 4.770 133 420.69 4.698 145 414.19 4.625 56 292.25 3.264 90 130.25 1.455 1000 123.81 1.383 946
in CDCl3
KBr disc
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