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MS-NW-5838 N,N,alpha-trimethylbenzylamine C10H15N (Mass of molecular ion: 149)
Source Temperature: 260 °C Sample Temperature: 190 °C Reservoir, 75 eV
15.0 1.9 18.0 1.1 27.0 2.1 39.0 2.1 42.0 7.1 44.0 5.2 45.0 1.2 50.0 1.4 51.0 4.0 56.0 2.5 63.0 1.1 65.0 1.4 72.0 34.0 73.0 1.8 77.0 8.7 78.0 2.8 79.0 4.4 91.0 5.2 103.0 4.0 104.0 3.5 105.0 17.0 106.0 2.2 118.0 3.7 132.0 1.2 134.0 100.0 135.0 10.8 148.0 2.2 149.0 8.8 150.0 1.1
90 MHz in CDCl3
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1H NMR 89.56 MHz C10 H15 N 0.04 ml : 0.5 ml CDCl3 N,N,alpha-trimethylbenzylamine Assign. Shift(ppm)
A 7.37 to 7.18 B 3.235 C 2.189 D 1.364 J(B,D)=6.7HZ.
Hz ppm Int.
655.00 7.314 25 654.19 7.305 42 652.06 7.281 317 650.94 7.269 97 649.63 7.254 62 293.44 3.277 36 286.75 3.202 38 196.06 2.190 1000 125.31 1.400 231 118.63 1.325 208
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