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网站主页CAS数据库列表 24463-15-8更多图谱1-芘甲醇(24463-15-8)质谱(MS)

1-芘甲醇

产品名称 1-芘甲醇

CAS号24463-15-8

分子式C17H12O

分子量232.28

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  • Mass

    MS-IW-7579          
    (1-pyrenyl)methanol
    C17H12O             (Mass of molecular ion:    232)
    

       Source Temperature: 170 °C
       Sample Temperature: 150 °C
       Direct, 75 eV
    

          17.0       1.2
          18.0       6.7
          87.0       2.0
          88.0       2.4
          93.5       3.0
          94.0       1.5
          94.5       6.2
          95.0       1.6
          99.0       1.4
          99.5       1.4
         100.0       8.1
         100.5       4.0
         101.0       7.2
         101.5       1.5
         102.0       2.9
         105.5       2.2
         106.0       2.1
         106.5       6.6
         107.0       4.0
         107.5       3.2
         108.0       3.0
         115.5       4.1
         116.0       2.5
         174.0       1.1
         187.0       1.7
         189.0       5.0
         198.0       1.5
         199.0       2.0
         200.0      10.9
         201.0      14.6
         202.0      31.7
         203.0      47.0
         204.0       9.8
         211.0       1.9
         212.0       1.2
         213.0       8.9
         214.0       4.8
         215.0      50.2
         216.0      30.7
         217.0       5.1
         229.0       5.4
         230.0       8.7
         231.0      14.3
         232.0     100.0
         233.0      18.3
         234.0       1.9
    

400 MHz at 60C


  • 1H NMR 399.65 MHz
    C17 H12 O saturated in CDCl3 at 60 C
    (1-pyrenyl)methanol
    ChemicalStructure
        Assign.     Shift(ppm)
    A 8.194 B 8.080 C 7.994 D 7.983 E 7.93 F 7.92 G 7.90 J 5.241 K 1.90

         Hz     ppm     Int.
    

       3279.91   8.207    388
       3270.75   8.185    488
       3233.40   8.091    654
       3229.98   8.083     45
       3229.49   8.081     46
       3225.71   8.072    786
       3199.71   8.007    322
       3194.58   7.994    497
       3192.02   7.988    491
       3187.99   7.977     37
       3185.42   7.971    393
       3179.20   7.955    186
       3170.29   7.933   1000
       3165.41   7.921    798
       3163.57   7.916    458
       3162.96   7.915    465
       3158.08   7.903    501
       3156.74   7.899    323
       3155.64   7.897    382
       3150.27   7.883    344
       2094.73   5.242    802
        760.01   1.902    222
    

in CDCl3



KBr disc



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