图谱信息 供应商 相关产品
网站主页CAS数据库列表 2432-14-6更多图谱2,6-二溴-4-甲基苯酚(2432-14-6)核磁图(1HNMR)

2,6-二溴-4-甲基苯酚

产品名称 2,6-二溴-4-甲基苯酚

CAS号2432-14-6

分子式C7H6Br2O

分子量265.93

展开


  • Mass

    MS2014-05027CW      
    2,6-dibromo-4-methylphenol
    C7H6Br2O            (Mass of molecular ion:    264)
    

       Source Temperature: 250 °C
       Sample Temperature:  25 °C
       Direct, 70 eV
    

          15.0       2.1
          17.0       6.7
          18.0       2.0
          25.0       1.4
          26.0       4.6
          27.0       9.4
          28.0       1.6
          29.0       3.4
          37.0       7.4
          38.0      16.0
          38.5       1.8
          39.0      10.8
          43.0       2.3
          49.0       6.0
          50.0      31.4
          51.0      58.1
          52.0      11.6
          52.5       1.7
          53.0      25.0
          54.0       1.4
          55.0       1.5
          60.0       1.2
          61.0       7.1
          62.0      10.4
          63.0       8.1
          65.0       1.1
          66.0       2.4
          73.0       3.6
          74.0      12.8
          75.0      17.1
          76.0      12.8
          77.0      68.7
          78.0      38.0
          79.0       7.7
          80.0       3.4
          81.0       5.8
          82.0       3.1
          83.0       1.0
          85.0       1.7
          86.0       2.2
          87.0       1.8
          92.0       1.1
          92.5       6.0
          93.0       1.7
          93.5       5.7
         104.0       2.5
         105.0      14.4
         106.0       9.6
         107.0       1.9
         117.0       1.3
         119.0       1.2
         129.0       1.3
         130.0       1.1
         131.0       2.1
         132.0       1.1
         133.0       2.5
         141.0       1.1
         143.0       1.1
         155.0       3.0
         156.0       4.8
         157.0       5.0
         158.0       4.7
         159.0       2.3
         183.0       3.6
         184.0       1.7
         185.0      80.7
         186.0       7.6
         187.0      75.1
         188.0       5.8
         263.0       6.6
         264.0      51.5
         265.0      16.9
         266.0     100.0
         267.0      14.1
         268.0      49.3
         269.0       3.8
    

90 MHz in CDCl3


  • 1H NMR 89.56 MHz
    C7 H6 Br2 O 0.047 g : 0.5 ml CDCl3
    2,6-dibromo-4-methylphenol
    ChemicalStructure
        Assign.     Shift(ppm)
    A 7.244 B 5.68 C 2.244

         Hz     ppm     Int.
    

        649.75   7.255    257
        649.06   7.248    447
        648.38   7.240    430
        509.00   5.684    388
        201.69   2.253    590
        201.00   2.245   1000
        200.31   2.237    523
    

in CDCl3



KBr disc



nujol mull