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MS-NW-9474 triphenylmethanesulfenyl chloride C19H15ClS (Mass of molecular ion: 310)
Source Temperature: 180 °C Sample Temperature: 120 °C Direct, 75 eV
64.0 1.9 113.0 1.1 115.0 1.2 119.5 2.0 120.0 1.3 139.0 1.2 163.0 1.5 164.0 1.8 165.0 34.1 166.0 5.8 167.0 1.3 202.0 2.0 213.0 1.3 215.0 4.4 216.0 1.0 226.0 3.1 227.0 1.8 228.0 7.7 229.0 1.6 237.0 1.6 238.0 1.1 239.0 12.1 240.0 5.0 241.0 20.8 242.0 18.0 243.0 100.0 244.0 22.7 245.0 2.5
400 MHz in CDCl3
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1H NMR 399.65 MHz C19 H15 Cl S 0.032 g : 0.5 ml CDCl3 triphenylmethanesulfenyl chloride Assign. Shift(ppm)
A 7.35 B 7.33 C 7.31 CONFIRMED BY LAOCN PROGRAM
Hz ppm Int.
2944.46 7.368 59 2942.99 7.364 81 2941.28 7.360 131 2940.43 7.358 155 2938.48 7.353 387 2937.13 7.350 307 2935.67 7.346 644 2934.57 7.343 684 2933.35 7.340 984 2931.03 7.334 857 2930.30 7.333 1000 2927.61 7.326 469 2926.03 7.322 363 2924.32 7.318 500 2922.97 7.314 263 2922.00 7.312 271 2920.53 7.308 161 2919.07 7.305 182 2914.67 7.294 116 2911.99 7.287 124 2906.86 7.274 30 2900.76 7.259 32
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