图谱信息 供应商 相关产品
网站主页CAS数据库列表 24106-05-6更多图谱4'-溴-2'-甲基乙酰苯胺(24106-05-6)红外图谱(IR2)

4'-溴-2'-甲基乙酰苯胺

产品名称 4'-溴-2'-甲基乙酰苯胺

CAS号24106-05-6

分子式C9H10BrNO

分子量228.09

展开


  • Mass

    MS2015-05116CW      
    4'-bromo-2'-methylacetanilide
    C9H10BrNO           (Mass of molecular ion:    227)
    

       Source Temperature: 245 °C
       Sample Temperature:  20 °C
       Direct, 70 eV
    

          17.0       1.2
          18.0       6.5
          39.0       1.5
          43.0      13.9
          44.0       2.4
          50.0       1.8
          51.0       4.5
          52.0       2.5
          57.0       1.2
          63.0       2.2
          75.0       1.3
          76.0       1.8
          77.0       8.8
          78.0       7.8
          79.0       4.5
          89.0       2.3
          90.0       1.5
         104.0       8.0
         105.0       5.9
         106.0      38.3
         107.0       4.2
         147.0       1.0
         149.0       2.0
         184.0      12.0
         185.0     100.0
         186.0      19.8
         187.0      99.9
         188.0       8.4
         227.0      43.2
         228.0       4.6
         229.0      41.8
         230.0       4.4
    

in CDCl3

400 MHz at 50C

400 MHz in DMSO-d6




  • 1H NMR 399.65 MHz
    C9 H10 Br N O 0.040 g : 0.5 ml CDCl3 at 50 C
    4'-bromo-2'-methylacetanilide
    ChemicalStructure
        Assign.     Shift(ppm)
    A 7.53 B 7.29 C 7.27 D 7.16 E 2.177 F 2.120

         Hz     ppm     Int.
    

       3010.01   7.532     34
       2914.55   7.293    148
       2908.45   7.278    136
       2899.54   7.256     90
       2863.16   7.165     32
        880.86   2.205     21
        870.00   2.177   1000
        847.41   2.121    201
    


  • 1H NMR 399.65 MHz
    C9 H10 Br N O 0.038 g : 0.5 ml DMSO-d6
    4'-bromo-2'-methylacetanilide
    ChemicalStructure
        Assign.     Shift(ppm)
    A 9.31 B 7.411 C 7.410 D 7.323 E 2.195 F 2.061

         Hz     ppm     Int.
    

       3719.33   9.307     91
       2966.46   7.423    107
       2963.10   7.415    165
       2961.12   7.410    180
       2958.22   7.403    163
       2931.37   7.335    108
       2929.23   7.330     99
       2922.82   7.314     69
       2920.53   7.308     64
        877.53   2.196   1000
        823.97   2.062    669
    

in CDCl3

in DMSO-d6





KBr disc



nujol mull