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MassMS-NW-6044 1,1-dichloro-1-silacyclohexane C5H10Cl2Si (Mass of molecular ion: 168)
Source Temperature: 260 °C Sample Temperature: 190 °C Reservoir, 75 eV
15.0 1.1 18.0 2.3 26.0 1.8 27.0 11.2 28.0 1.5 29.0 5.1 36.0 2.4 38.0 1.7 39.0 20.4 40.0 3.7 41.0 31.4 42.0 18.4 43.0 10.7 44.0 1.4 47.0 1.0 51.0 1.2 53.0 2.6 54.0 10.5 55.0 11.9 56.0 2.3 57.0 3.3 63.0 29.8 64.0 2.8 65.0 11.8 66.0 1.5 67.0 3.4 68.0 2.5 69.0 15.4 70.0 8.5 71.0 1.8 77.0 2.3 78.0 1.6 79.0 2.0 80.0 1.6 81.0 1.0 90.0 1.0 91.0 1.7 93.0 1.6 95.0 2.0 96.0 2.7 97.0 2.0 98.0 11.2 99.0 19.1 100.0 8.4 101.0 12.8 102.0 2.2 103.0 3.7 104.0 7.5 105.0 3.7 106.0 3.2 107.0 1.7 108.0 2.0 109.0 1.1 111.0 1.6 112.0 56.9 113.0 14.1 114.0 38.2 115.0 9.0 116.0 7.8 117.0 5.9 119.0 2.0 123.0 1.1 124.0 2.0 125.0 27.5 126.0 13.7 127.0 56.2 128.0 12.2 129.0 30.4 130.0 4.1 131.0 6.6 132.0 29.0 133.0 6.0 134.0 10.5 135.0 2.4 136.0 2.3 137.0 1.1 138.0 1.2 139.0 12.9 140.0 100.0 141.0 16.7 142.0 66.2 143.0 7.7 144.0 12.3 145.0 1.5 152.0 1.3 153.0 2.8 155.0 1.8 161.0 1.4 163.0 1.2 167.0 1.2 168.0 42.7 169.0 5.4 170.0 28.2 171.0 3.6 172.0 5.6
400 MHz in CDCl3
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1H NMR 399.65 MHz C5 H10 Cl2 Si 0.05 ml : 0.5 ml CDCl3 1,1-dichloro-1-silacyclohexane 
Assign. Shift(ppm)
A 1.839 B 1.497 C 1.197
Hz ppm Int.747.56 1.871 271 741.82 1.857 389 740.97 1.855 405 739.01 1.850 347 738.28 1.848 374 735.96 1.842 549 734.50 1.838 511 731.69 1.831 373 731.08 1.830 367 729.61 1.826 403 728.64 1.824 409 722.66 1.809 278 609.50 1.526 187 606.81 1.519 145 605.47 1.516 110 603.76 1.511 285 601.07 1.504 203 598.14 1.497 481 595.46 1.490 194 594.24 1.487 154 592.77 1.484 205 592.04 1.482 188 589.72 1.476 123 586.79 1.469 143 485.23 1.215 1000 480.83 1.204 372 478.39 1.198 983 471.68 1.181 862
in CDCl3
liquid film
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