-
MassMS-IW-0800 3-benzyloxy-2-pyridinamine C12H12N2O (Mass of molecular ion: 200)
Source Temperature: 110 °C Sample Temperature: 80 °C Direct, 75 eV
39.0 2.7 65.0 5.6 81.0 2.9 91.0 100.0 92.0 8.0 106.0 2.4 109.0 4.9 183.0 5.6 184.0 1.3 199.0 6.5 200.0 50.2 201.0 7.3
400 MHz in CDCl3
-
1H NMR 399.65 MHz C12 H12 N2 O 0.037 g : 0.5 ml CDCl3 3-benzyloxy-2-pyridinamine 
Assign. Shift(ppm)
A 7.669 B 7.40 C 7.35 D 6.941 E 6.571 F 5.043 G 4.8
Hz ppm Int.3068.24 7.678 197 3066.89 7.674 206 3063.23 7.665 212 3061.89 7.662 208 2966.55 7.423 41 2964.11 7.417 82 2961.55 7.411 57 2957.89 7.402 732 2956.05 7.397 438 2952.03 7.387 374 2951.29 7.385 471 2949.10 7.380 113 2947.39 7.375 50 2945.68 7.371 106 2944.34 7.368 135 2943.48 7.366 147 2941.04 7.360 119 2938.72 7.354 142 2935.91 7.347 108 2933.35 7.340 93 2932.25 7.338 112 2928.10 7.327 44 2926.39 7.323 37 2925.78 7.321 33 2779.05 6.954 167 2777.71 6.951 169 2771.24 6.935 190 2769.90 6.931 188 2632.57 6.588 226 2627.56 6.575 226 2624.88 6.568 210 2619.75 6.556 208 2015.50 5.044 1000 1913.45 4.788 100
in CDCl3
KBr disc
nujol mull
更多供应商
