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MS-NW-3438 p-methoxybenzylamine C8H11NO (Mass of molecular ion: 137)
Source Temperature: 270 °C Sample Temperature: 180 °C Reservoir, 75 eV
15.0 7.5 18.0 1.6 26.0 1.8 27.0 4.3 28.0 24.4 29.0 3.9 30.0 28.6 31.0 1.1 37.0 3.2 38.0 7.2 39.0 16.4 40.0 3.1 41.0 7.2 42.0 2.4 44.0 1.1 49.0 1.3 50.0 10.8 51.0 15.7 52.0 7.8 53.0 3.8 54.0 3.0 55.0 1.4 61.0 2.2 62.0 5.2 63.0 12.6 64.0 8.8 65.0 14.5 66.0 12.1 67.0 7.8 68.0 1.4 74.0 3.5 75.0 2.6 76.0 3.5 77.0 26.7 78.0 19.4 79.0 9.3 80.0 1.5 81.0 1.0 89.0 6.0 90.0 4.7 91.0 11.4 92.0 6.9 93.0 17.5 94.0 18.4 95.0 3.4 103.0 1.9 104.0 7.2 105.0 6.8 106.0 42.3 107.0 6.0 108.0 8.3 109.0 20.3 110.0 1.6 119.0 4.9 120.0 11.2 121.0 59.1 122.0 13.7 123.0 1.0 133.0 4.6 134.0 4.9 135.0 2.3 136.0 100.0 137.0 49.0 138.0 4.7 150.0 1.2 255.0 1.4
90 MHz in CDCl3
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1H NMR 89.56 MHz C8 H11 N O 0.04 ml : 0.5 ml CDCl3 p-methoxybenzylamine Assign. Shift(ppm)
A 7.20 B 6.86 C 3.77 D 3.759 E 1.41
Hz ppm Int.
649.63 7.254 107 647.38 7.229 35 643.00 7.180 60 641.31 7.161 158 640.81 7.156 168 638.63 7.131 22 638.13 7.126 23 619.75 6.920 28 617.13 6.891 213 614.81 6.865 55 610.44 6.816 50 608.38 6.793 118 336.69 3.760 1000 126.13 1.409 204
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