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MS-IW-7682 alpha-bromo-2,4-difluorotoluene C7H5BrF2 (Mass of molecular ion: 206)
Source Temperature: 220 °C Sample Temperature: 150 °C Reservoir, 75 eV
50.0 1.2 51.0 1.5 57.0 2.2 63.0 1.1 75.0 2.3 77.0 2.7 81.0 1.8 93.0 1.2 94.0 1.1 101.0 7.6 107.0 4.4 125.0 3.8 126.0 2.7 127.0 100.0 128.0 7.7 206.0 2.4 208.0 2.3
400 MHz in CDCl3
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1H NMR 399.65 MHz C7 H5 Br F2 0.05 ml : 0.5 ml CDCl3 alpha-bromo-2,4-difluorotoluene Assign. Shift(ppm)
A 7.358 B 6.86 C 6.81 D 4.472
Hz ppm Int.
2952.51 7.388 101 2952.15 7.387 102 2946.17 7.372 113 2943.97 7.367 218 2937.62 7.351 219 2935.30 7.345 130 2929.08 7.330 119 2750.24 6.882 80 2749.02 6.879 81 2747.68 6.876 98 2746.58 6.873 101 2740.97 6.859 131 2738.40 6.852 176 2732.67 6.838 203 2730.10 6.832 190 2723.88 6.816 168 2723.02 6.814 176 2721.68 6.811 130 2720.46 6.808 138 2714.23 6.792 138 2711.67 6.786 114 1786.99 4.472 1000
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