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3,5-二叔丁基苯胺

产品名称 3,5-二叔丁基苯胺

CAS号2380-36-1

分子式C14H23N

分子量205.34

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  • Mass

    MS-IW-9450          
    3,5-di-tert-butylaniline
    C14H23N             (Mass of molecular ion:    205)
    

       Source Temperature: 220 °C
       Sample Temperature: 150 °C
       Reservoir, 75 eV
    

          27.0       1.6
          28.0       2.2
          29.0       9.9
          30.0       1.0
          39.0       3.7
          41.0      16.1
          42.0       2.1
          51.0       1.6
          53.0       1.8
          55.0       2.9
          57.0      61.3
          58.0       2.9
          58.5       2.6
          59.5       5.8
          63.0       1.0
          64.5       1.8
          65.0       4.3
          65.5       4.8
          66.0       1.7
          67.0       1.2
          71.5       3.6
          72.0       1.4
          72.5       7.3
          73.0       1.3
          73.5      11.2
          74.0       1.3
          77.0       4.1
          78.0       1.3
          79.0       1.9
          87.0       1.4
          87.5       8.8
          88.0       1.2
          91.0       4.9
          92.0       1.1
          93.0       4.8
          94.0       7.4
          95.0       3.7
         103.0       1.3
         105.0       1.8
         106.0       7.6
         107.0       5.3
         108.0       1.2
         115.0       3.5
         116.0       1.7
         117.0       3.9
         118.0       3.1
         119.0       2.9
         120.0       3.3
         121.0       1.0
         128.0       1.4
         129.0       1.0
         130.0       3.4
         131.0       2.6
         132.0       4.4
         133.0       2.8
         134.0      78.3
         135.0       8.4
         143.0       1.5
         144.0       2.2
         145.0       1.9
         146.0       2.7
         147.0       3.5
         148.0       7.2
         149.0       1.7
         158.0       1.0
         159.0       1.0
         160.0       1.9
         162.0       6.5
         163.0      15.6
         164.0       2.0
         174.0       2.4
         175.0       1.0
         190.0      98.6
         191.0      14.5
         192.0       1.0
         204.0       1.7
         205.0     100.0
         206.0      16.1
         207.0       1.2
    

400 MHz in CDCl3


  • 1H NMR 399.65 MHz
    C14 H23 N 0.041 g : 0.5 ml CDCl3
    3,5-di-tert-butylaniline
    ChemicalStructure
        Assign.     Shift(ppm)
    A 6.845 B 6.557 C 3.6 D 1.287

         Hz     ppm     Int.
    

       2737.30   6.850     36
       2735.60   6.845     65
       2733.89   6.841     37
       2621.34   6.560    139
       2619.75   6.556    134
        514.65   1.288   1000
    

in CDCl3



KBr disk



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