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MassMS-NW-9131 4-bromo-2,6-xylenol C8H9BrO (Mass of molecular ion: 200)
Source Temperature: 260 °C Sample Temperature: 150 °C Reservoir, 75 eV
27.0 3.5 38.0 1.7 39.0 9.1 40.0 1.1 41.0 3.5 43.0 3.9 45.0 4.5 46.0 2.3 50.0 3.3 51.0 9.4 52.0 3.1 53.0 5.7 55.0 2.2 59.0 1.5 60.0 2.2 60.5 1.3 61.0 1.0 62.0 2.2 63.0 5.2 64.0 1.5 65.0 11.0 66.0 1.7 67.0 1.3 74.0 1.1 75.0 1.4 76.0 1.1 77.0 39.3 78.0 7.9 79.0 1.6 89.0 2.0 90.0 1.4 91.0 39.1 92.0 16.6 93.0 10.3 94.0 1.1 99.0 1.1 100.0 2.6 101.0 1.8 102.0 2.6 103.0 16.7 104.0 2.1 107.0 2.2 119.0 1.2 120.0 1.8 121.0 100.0 122.0 10.9 171.0 1.0 182.0 1.1 184.0 1.1 185.0 3.8 187.0 3.3 199.0 6.5 200.0 93.5 201.0 14.4 202.0 90.9 203.0 8.0
90 MHz in CDCl3
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1H NMR 89.56 MHz C8 H9 Br O 0.047 g : 0.5 ml CDCl3 4-bromo-2,6-xylenol 
Assign. Shift(ppm)
A 7.081 B 4.6 C 2.196
Hz ppm Int.634.88 7.089 148 634.25 7.082 199 633.56 7.075 156 197.31 2.204 554 196.69 2.197 1000 196.06 2.190 560
in CDCl3
KBr disc
Nujol
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