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MS-IW-2632 4-amino-3-hydroxybenzoic acid C7H7NO3 (Mass of molecular ion: 153)
Source Temperature: 130 °C Sample Temperature: 90 °C Direct, 75 eV
18.0 3.3 28.0 2.4 39.0 1.8 40.0 1.0 41.0 1.1 50.0 1.9 51.0 3.4 52.0 4.7 53.0 6.8 53.5 1.8 54.0 2.5 62.0 1.2 62.5 3.6 63.0 3.3 68.0 2.0 78.0 2.3 79.0 2.8 80.0 13.2 81.0 1.0 90.0 1.1 96.0 2.0 107.0 2.1 108.0 11.7 109.0 1.0 124.0 2.2 136.0 71.6 137.0 6.0 138.0 1.1 152.0 2.3 153.0 100.0 154.0 8.1
400 MHz in DMSO-d6
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1H NMR 399.65 MHz C7 H7 N O3 0.039 g : 0.5 ml DMSO-d6 4-amino-3-hydroxybenzoic acid Assign. Shift(ppm)
A *1 12. B *1 9.36 C 7.273 D 7.263 E 6.604 F 5.3
Hz ppm Int.
3738.79 9.356 63 2907.04 7.274 1000 2905.57 7.271 533 2900.08 7.257 339 2898.24 7.252 266 2643.83 6.616 355 2642.18 6.612 164 2636.86 6.598 109 2635.03 6.594 346
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