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MS-IW-6666 4,4'-diamino-3,3'-biphenyldiol C12H12N2O2 (Mass of molecular ion: 216)
Source Temperature: 180 °C Sample Temperature: 210 °C Direct, 75 eV
71.5 1.5 79.0 1.3 80.0 1.3 93.5 2.6 94.0 1.1 108.0 10.9 108.5 1.5 109.0 1.5 115.0 2.4 126.0 1.0 142.0 1.1 143.0 1.9 154.0 1.0 170.0 1.8 171.0 1.8 172.0 1.2 187.0 12.6 188.0 1.9 197.0 1.7 198.0 1.2 215.0 2.1 216.0 100.0 217.0 14.0 218.0 1.3
400 MHz in DMSO-d6
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1H NMR 399.65 MHz C12 H12 N2 O2 0.041 g : 0.5 ml DMSO-d6 4,4'-diamino-3,3'-biphenyldiol Assign. Shift(ppm)
A 9.0 B 6.823 C 6.714 D 6.601 E 4.5
Hz ppm Int.
3606.41 9.024 67 2738.34 6.852 21 2727.97 6.826 960 2726.14 6.822 978 2714.39 6.792 24 2712.40 6.787 21 2688.75 6.728 464 2686.92 6.724 426 2680.66 6.708 627 2678.83 6.703 584 2641.60 6.610 1000 2633.67 6.590 741 1785.74 4.469 168
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