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MS-NW-9481 N,N'-methylenebis(methacrylamide) C9H14N2O2 (Mass of molecular ion: 182)
Source Temperature: 190 °C Sample Temperature: 110 °C Direct, 75 eV
18.0 3.7 28.0 3.3 30.0 3.8 39.0 8.8 40.0 2.7 41.0 41.0 42.0 3.1 43.0 1.4 44.0 1.7 45.0 1.1 46.0 18.5 55.0 1.5 58.0 1.4 68.0 5.7 69.0 100.0 70.0 7.1 85.0 3.0 86.0 14.5 96.0 2.5 97.0 17.2 98.0 7.8 113.0 67.2 114.0 4.5 182.0 2.2
400 MHz in DMSO-d6
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1H NMR 399.65 MHz C9 H14 N2 O2 0.030 g : 0.5 ml DMSO-d6 N,N'-methylenebis(methacrylamide) Assign. Shift(ppm)
A 8.38 B 5.716 C 5.372 D 4.568 E 1.852 J(A,D)=5.1HZ
Hz ppm Int.
3352.66 8.389 61 3347.47 8.377 106 3342.44 8.364 67 2284.70 5.717 305 2148.59 5.377 204 2147.06 5.373 281 2145.84 5.370 221 1831.51 4.583 107 1825.71 4.569 205 1819.92 4.554 116 740.20 1.853 1000
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