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网站主页CAS数据库列表 2344-70-9更多图谱4-苯基-2-丁醇(2344-70-9)质谱(MS)

4-苯基-2-丁醇

产品名称 4-苯基-2-丁醇

CAS号2344-70-9

分子式C10H14O

分子量150.22

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  • Mass

    MS-NW-5683          
    4-phenyl-2-butanol
    C10H14O             (Mass of molecular ion:    150)
    

       Source Temperature: 260 °C
       Sample Temperature: 190 °C
       Reservoir, 75 eV
    

          15.0       1.1
          19.0       1.0
          27.0       5.5
          28.0       1.5
          29.0       1.7
          31.0       1.9
          38.0       1.0
          39.0       8.3
          41.0       2.9
          43.0       7.5
          45.0      33.3
          50.0       3.4
          51.0       9.9
          52.0       2.8
          53.0       1.9
          54.0       2.4
          55.0       1.0
          57.0       1.6
          58.0       1.1
          59.0       2.6
          62.0       1.3
          63.0       4.3
          64.0       1.4
          65.0      13.4
          66.0       1.0
          72.0       1.0
          74.0       1.2
          75.0       1.2
          76.0       1.0
          77.0      13.4
          78.0      26.1
          79.0       9.8
          89.0       3.2
          90.0       1.5
          91.0      96.3
          92.0      48.0
          93.0       4.0
         102.0       1.2
         103.0       6.6
         104.0       6.3
         105.0      14.1
         106.0       3.7
         107.0       1.1
         115.0       5.8
         116.0       2.2
         117.0     100.0
         118.0      10.5
         129.0       1.0
         131.0       9.7
         132.0      67.3
         133.0       8.0
         135.0       1.0
         148.0       1.0
         150.0       8.6
         151.0       1.1
    

400 MHz in CDCl3


  • 1H NMR 399.65 MHz
    C10 H14 O 0.05 ml : 0.5 ml CDCl3
    4-phenyl-2-butanol
    ChemicalStructure
        Assign.     Shift(ppm)
    A 7.248 B 7.17 C 7.15 D 3.772 E *1 2.717 F *1 2.635 G 2.39 J *2 1.752 K *2 1.715 L 1.187 J(E,K)=9.7HZ J(E,F)=-13.8HZ J(E,J)=6.1HZ J(F,K)=6.8HZ J(F,J)=9.4HZ J(J.K)=-13.6HZ J(J,D)=7.5HZ J(K,D)=5.1HZ

         Hz     ppm     Int.
    

       2905.76   7.271    104
       2904.91   7.269    156
       2903.32   7.265     84
       2898.32   7.253    255
       2897.46   7.250    314
       2892.21   7.237    127
       2890.26   7.232    325
       2885.86   7.221     31
       2876.71   7.199     30
       2869.63   7.181    416
       2866.94   7.174    205
       2865.72   7.171    199
       2862.67   7.163    260
       2862.18   7.162    254
       2858.52   7.153    215
       2856.45   7.148     78
       2852.66   7.138     61
       2851.32   7.135     85
       2850.10   7.132     53
       1515.38   3.792     37
       1510.38   3.780     63
       1504.27   3.764     64
       1499.76   3.753     37
       1499.15   3.752     37
       1103.15   2.761     40
       1097.05   2.746     46
       1093.51   2.737     46
       1089.36   2.726     87
       1087.52   2.722     58
       1083.37   2.711     87
       1079.71   2.702     93
       1073.61   2.687     89
       1066.16   2.668     85
       1059.33   2.651     98
       1056.64   2.644     90
       1052.37   2.634     51
       1049.93   2.628     93
       1045.53   2.617     48
       1042.97   2.610     47
       1036.13   2.593     44
        954.59   2.389    143
        716.92   1.794     36
        715.58   1.791     31
        713.50   1.786     31
        709.47   1.776    110
        707.40   1.771     41
        706.30   1.768     35
        703.37   1.760     93
        702.03   1.757    103
        699.95   1.752    124
        698.49   1.748    103
        695.92   1.742     98
        693.60   1.736    153
        692.63   1.734    138
        691.77   1.731    124
        688.72   1.724     93
        686.52   1.718    173
        684.94   1.714     59
        683.59   1.711     94
        682.01   1.707     89
        679.81   1.702     39
        677.98   1.697     41
        676.88   1.694     86
        675.17   1.690     40
        670.04   1.677     31
        481.45   1.205     57
        477.54   1.195    967
        474.49   1.188     83
        471.31   1.180   1000
        467.65   1.171     46
    

in CDCl3



liquid film