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MassMS-NW-6324 1-acetylthiosemicarbazide C3H7N3OS (Mass of molecular ion: 133)
Source Temperature: 160 °C Sample Temperature: 100 °C Direct, 75 eV
14.0 1.3 15.0 7.9 18.0 2.6 27.0 1.3 28.0 9.2 29.0 1.9 31.0 8.4 32.0 68.0 33.0 1.5 41.0 1.2 42.0 5.1 43.0 68.8 44.0 3.7 45.0 1.4 47.0 1.3 48.0 1.7 56.0 1.5 57.0 1.2 58.0 3.0 59.0 3.8 60.0 39.9 61.0 1.9 62.0 2.1 74.0 35.1 75.0 1.6 91.0 14.5 100.0 15.6 116.0 7.7 133.0 100.0 134.0 5.7 135.0 4.9
400 MHz in DMSO-d6
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1H NMR 399.65 MHz C3 H7 N3 O S 0.039 g : 0.5 ml DMSO-d6 1-acetylthiosemicarbazide 
Assign. Shift(ppm)
A *1 9.72 B *1 9.15 C *2 7.82 D *2 7.48 E 1.832
Hz ppm Int.3883.82 9.719 113 3657.23 9.152 85 3124.69 7.819 47 3124.39 7.818 47 2989.35 7.480 54 732.27 1.833 1000 722.96 1.809 129
in DMSO-d6
KBr disc
nujol mull
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