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MassMS-NW-7434 1-(p-methoxyphenyl)thiourea C8H10N2OS (Mass of molecular ion: 182)
Source Temperature: 170 °C Sample Temperature: 160 °C Direct, 75 eV
15.0 2.1 18.0 2.3 26.0 1.8 27.0 2.9 28.0 5.6 32.0 2.1 33.0 1.0 34.0 1.4 37.0 1.8 38.0 3.8 39.0 7.5 40.0 1.0 41.0 5.3 43.0 4.4 45.0 1.7 50.0 5.0 51.0 6.7 52.0 12.4 53.0 12.0 54.0 2.7 59.0 2.7 60.0 18.2 61.0 1.9 62.0 3.4 63.0 9.8 64.0 8.2 65.0 6.7 66.0 1.3 67.0 1.2 69.0 1.1 70.0 1.3 74.0 1.9 75.0 1.6 76.0 1.9 77.0 9.5 78.0 4.6 79.0 4.1 80.0 21.3 81.0 2.8 90.0 2.6 91.0 2.0 92.0 6.7 93.0 1.1 95.0 6.3 96.0 2.7 97.0 1.5 105.0 3.6 106.0 1.4 107.0 4.0 108.0 100.0 109.0 8.0 110.0 1.0 122.0 13.0 123.0 33.7 124.0 3.3 125.0 4.5 133.0 8.3 134.0 4.1 138.0 1.2 139.0 1.4 140.0 43.5 141.0 4.0 142.0 2.6 148.0 6.5 149.0 24.5 150.0 14.1 151.0 1.6 165.0 16.4 166.0 4.5 167.0 2.0 181.0 1.3 182.0 62.5 183.0 7.8 184.0 3.5
90 MHz in DMSO-d6
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1H NMR 89.56 MHz C8 H10 N2 O S 0.036 g : 0.5 ml DMSO-d6 1-(p-methoxyphenyl)thiourea 
Assign. Shift(ppm)
A *1 9.47 B *1 7.2 C 7.24 D 6.908 E 3.734
Hz ppm Int.848.73 9.477 141 848.22 9.471 140 652.88 7.290 173 650.61 7.265 109 643.80 7.189 238 625.05 6.980 42 621.97 6.945 249 619.56 6.918 71 617.58 6.896 26 617.14 6.891 26 615.23 6.870 59 612.82 6.843 139 334.50 3.735 1000
DMSO-d6
KBr disc
nujol mull
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