-
MassMS-IW-7683 (R)-(1-ethyl-2-pyrrolidinyl)methylamine C7H16N2 (Mass of molecular ion: 128)
Source Temperature: 220 °C Sample Temperature: 150 °C Reservoir, 75 eV
27.0 2.4 28.0 9.1 29.0 2.7 30.0 3.7 39.0 1.5 41.0 5.1 42.0 2.9 43.0 6.8 44.0 1.2 54.0 1.4 55.0 2.0 56.0 4.3 67.0 1.1 68.0 4.5 69.0 1.6 70.0 21.2 71.0 1.7 80.0 1.6 82.0 2.9 95.0 1.0 96.0 4.2 97.0 1.9 98.0 100.0 99.0 7.5
400 MHz in CDCl3
-
1H NMR 399.65 MHz C7 H16 N2 0.05 ml : 0.5 ml CDCl3 (R)-(1-ethyl-2-pyrrolidinyl)methylamine 
Assign. Shift(ppm)
A 3.152 B *1 2.821 C *2 2.722 D *2 2.675 E 2.367 F *1 2.205 G 2.136 J 2.05 K 1.880 L *3 1.74 M *3 1.71 P 1.604 Q 1.097 ASSIGNED BY C-H COSY
Hz ppm Int.1269.90 3.178 62 1264.77 3.165 106 1260.38 3.154 119 1255.25 3.141 99 1251.10 3.131 71 1145.14 2.866 36 1137.70 2.847 106 1133.18 2.836 48 1130.25 2.829 112 1125.73 2.817 119 1122.92 2.810 48 1118.41 2.799 119 1110.96 2.780 43 1099.49 2.752 77 1095.70 2.742 88 1086.79 2.720 228 1082.89 2.710 238 1075.81 2.692 214 1069.70 2.677 228 1062.99 2.660 72 1057.01 2.645 86 958.37 2.399 38 954.59 2.389 40 951.90 2.382 65 950.07 2.378 59 948.24 2.373 69 946.04 2.368 76 943.73 2.362 76 942.02 2.358 55 939.94 2.352 70 937.50 2.346 45 933.59 2.337 37 897.71 2.247 47 890.63 2.229 141 885.74 2.217 54 883.54 2.211 151 878.78 2.199 136 876.59 2.194 67 871.70 2.182 139 867.07 2.170 85 864.62 2.164 58 858.28 2.148 194 849.73 2.127 200 840.94 2.105 100 819.58 2.051 240 771.36 1.931 37 763.43 1.911 89 759.40 1.901 46 755.25 1.890 112 752.56 1.884 65 750.85 1.879 69 746.83 1.869 57 743.29 1.860 84 741.94 1.857 60 734.86 1.839 65 704.22 1.763 54 701.66 1.756 56 698.12 1.747 115 695.92 1.742 138 693.60 1.736 76 691.28 1.730 144 689.58 1.726 137 688.60 1.724 155 687.50 1.721 197 682.86 1.709 214 679.32 1.700 109 674.56 1.688 101 655.03 1.640 56 650.51 1.628 36 648.56 1.623 70 646.73 1.619 49 643.43 1.610 68 640.38 1.603 49 636.23 1.592 80 630.98 1.579 33 629.27 1.575 67 445.80 1.116 610 438.48 1.098 1000 431.40 1.080 631
in CDCl3
liquid film
更多供应商
