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MS-IW-0204 5-chloromethyl-2-oxazolidinone C4H6ClNO2 (Mass of molecular ion: 135)
Source Temperature: 250 °C Sample Temperature: 160 °C Reservoir, 75 eV
15.0 3.3 18.0 1.3 27.0 3.9 28.0 12.7 29.0 6.8 30.0 5.6 42.0 18.2 43.0 5.2 44.0 1.1 49.0 1.4 54.0 1.0 56.0 2.1 58.0 5.8 79.0 2.9 86.0 100.0 87.0 3.9 135.0 12.4 136.0 2.1 137.0 4.1
400 MHz in DMSO-d6
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1H NMR 399.65 MHz C4 H6 Cl N O2 0.035 g : 0.5 ml DMSO-d6 5-chloromethyl-2-oxazolidinone Assign. Shift(ppm)
A 7.61 B 4.840 C *1 3.877 D *1 3.812 E *2 3.588 F *2 3.256
Hz ppm Int.
3042.72 7.614 263 1946.66 4.871 170 1942.63 4.861 214 1941.77 4.859 255 1940.55 4.856 230 1937.62 4.849 345 1936.52 4.846 295 1935.67 4.844 294 1933.59 4.839 256 1932.74 4.837 312 1931.64 4.834 362 1928.71 4.826 230 1927.49 4.823 244 1926.64 4.821 255 1922.61 4.811 187 1559.81 3.903 419 1555.79 3.893 415 1547.85 3.874 899 1543.95 3.864 864 1529.79 3.828 1000 1524.90 3.816 967 1517.82 3.798 478 1513.06 3.786 463 1443.73 3.613 379 1443.12 3.611 402 1434.69 3.590 800 1434.08 3.589 838 1425.54 3.567 413 1424.93 3.566 438 1309.08 3.276 391 1308.11 3.274 424 1302.86 3.261 387 1302.00 3.258 436 1299.93 3.253 376 1299.07 3.251 374 1293.82 3.238 347 1292.85 3.235 364
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