异戊醛-DNPH

产品名称异戊醛-DNPH

CAS号2256-01-1

分子式C11H14N4O4

分子量266.25

¹³CNMR

Mass

MS-IW-8134          
isovaleraldehyde 2,4-dinitrophenylhydrazone
C11H14N4O4          (Mass of molecular ion:    266)

   Source Temperature: 160 °C
   Sample Temperature: 140 °C
   Direct, 75 eV

      15.0       1.2
      26.0       1.1
      27.0      34.3
      28.0      13.8
      29.0      19.6
      30.0      23.1
      37.0       1.0
      38.0       3.9
      39.0      17.1
      40.0       3.3
      41.0      54.7
      42.0       9.8
      43.0      86.8
      44.0       4.5
      45.0       3.7
      50.0       5.0
      51.0      14.5
      52.0       9.1
      53.0       5.9
      54.0       2.6
      55.0      29.9
      56.0      21.0
      57.0      11.5
      58.0       2.2
      61.0       1.6
      62.0       7.4
      63.0      18.9
      64.0      12.8
      65.0       7.8
      66.0       3.5
      67.0       6.1
      68.0       8.9
      69.0      45.7
      70.0       4.2
      71.0       1.1
      74.0       4.4
      75.0      20.9
      76.0      13.7
      77.0      32.8
      78.0      22.5
      79.0      23.9
      80.0       5.2
      81.0       1.7
      82.0       4.7
      83.0       2.9
      84.0       4.7
      85.0       1.4
      87.0       4.0
      88.0       1.9
      89.0       4.6
      90.0       8.6
      91.0      11.1
      92.0      17.0
      93.0       4.4
      94.0       1.2
      95.0       1.2
     102.0       6.2
     103.0      23.2
     104.0      19.8
     105.0       8.1
     106.0       4.6
     107.0       3.3
     108.0       1.7
     115.0       1.8
     116.0       2.9
     117.0       4.3
     118.0       5.2
     119.0       6.9
     120.0       3.5
     121.0       1.9
     122.0      29.4
     123.0       2.5
     128.0       1.2
     129.0       2.8
     130.0       8.0
     131.0       8.5
     132.0       5.1
     133.0       2.3
     134.0       1.6
     135.0       2.7
     136.0       1.6
     137.0       3.1
     138.0       4.3
     143.0       1.7
     144.0       2.4
     145.0       2.1
     146.0       1.4
     147.0       5.1
     148.0       2.7
     149.0      22.7
     150.0       9.1
     151.0       3.0
     152.0      31.1
     153.0       6.7
     156.0       1.4
     157.0       3.2
     158.0       2.4
     159.0       2.1
     160.0       3.3
     161.0       2.2
     162.0       5.1
     163.0       2.8
     164.0       4.4
     165.0       5.7
     166.0       4.6
     167.0       5.6
     168.0       1.7
     172.0       2.5
     173.0       1.3
     176.0       8.1
     177.0      21.1
     178.0       4.8
     179.0       2.1
     180.0      19.7
     181.0       5.8
     183.0      26.8
     184.0       8.1
     185.0       7.7
     186.0       1.6
     189.0       1.7
     190.0       5.7
     191.0       4.0
     192.0       1.3
     193.0      37.3
     194.0       3.8
     196.0      24.4
     197.0       2.2
     202.0       2.5
     203.0       6.2
     204.0       3.0
     205.0       2.5
     206.0      37.6
     207.0      18.9
     208.0       4.0
     209.0       1.5
     210.0       2.3
     216.0       1.9
     217.0       1.3
     218.0       1.2
     223.0      23.0
     224.0      23.5
     225.0       2.6
     231.0      15.5
     232.0       3.0
     233.0       7.0
     234.0       1.6
     248.0       1.2
     249.0       1.4
     250.0       3.3
     251.0       4.6
     265.0       1.5
     266.0     100.0
     267.0      21.8
     268.0       2.7

400 MHz in CDCl3

¹H NMR	399.65 MHz
C₁₁ H₁₄ N₄ O₄	0.032 g : 0.5 ml CDCl₃
isovaleraldehyde 2,4-dinitrophenylhydrazone

    Assign.     Shift(ppm)

      A            11.0
      B             9.103
      C             8.289
      D             7.938
      E             7.561
      F             2.332
      G             1.990
      J             1.031

     Hz     ppm     Int.

   4411.46  11.039     63
   3639.53   9.107    176
   3636.93   9.101    181
   3319.70   8.307     58
   3318.94   8.305     63
   3317.11   8.301     59
   3316.35   8.299     60
   3310.09   8.283     68
   3309.33   8.281     72
   3307.50   8.276     70
   3306.73   8.275     70
   3177.19   7.950    153
   3167.57   7.926    134
   3027.65   7.576     56
   3021.85   7.562    114
   3016.05   7.547     58
    938.72   2.349    153
    932.92   2.335    183
    931.85   2.332    201
    926.06   2.318    174
    802.31   2.008     53
    795.44   1.991     65
    788.73   1.974     53
    415.50   1.040   1000
    408.78   1.023    985

in CDCl3

KBr disc

nujol mull

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异戊醛-DNPH(2256-01-1)质谱(MS) 相关产品图谱

丙醛2,4-二硝基苯肼(725-00-8)质谱(MS) 丙醛2,4-二硝基苯肼(725-00-8)红外图谱(IR1) 丙醛2,4-二硝基苯肼(725-00-8)红外图谱(IR2) 异戊醛-DNPH(2256-01-1)核磁图(¹³CNMR) 异戊醛-DNPH(2256-01-1)核磁图(¹HNMR)

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