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苯甲酮二甲基缩酮

产品名称 苯甲酮二甲基缩酮

CAS号2235-01-0

分子式C15H16O2

分子量228.29

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  • Mass

    MS-KW-0283          
    benzophenone dimethyl acetal
    C15H16O2            (Mass of molecular ion:    228)
    

       Source Temperature: 230 °C
       Sample Temperature: 150 °C
       Reservoir, 75 eV
    

          15.0       2.4
          29.0       1.9
          31.0       1.8
          39.0       1.3
          45.0       1.0
          50.0       3.6
          51.0      14.1
          52.0       1.0
          59.0       4.3
          63.0       1.4
          65.0       1.0
          74.0       1.8
          75.0       1.5
          76.0       4.7
          77.0      55.7
          78.0       4.0
          82.5       2.0
          91.0       7.3
          92.0       1.1
         105.0      83.7
         106.0       6.5
         151.0      28.2
         152.0       6.4
         153.0       2.5
         154.0       2.3
         165.0       3.4
         181.0       4.1
         182.0      20.6
         183.0       3.0
         197.0     100.0
         198.0      15.6
         199.0       1.3
    

400 MHz in CDCl3


  • 1H NMR 399.65 MHz
    C15H16O2 0.038 g : 0.5 ml CDCl3
    benzophenone dimethyl acetal
    ChemicalStructure
        Assign.     Shift(ppm)
    A 7.498 B 7.279 C 7.208 D 3.121

         Hz     ppm     Int.
    

       3003.91   7.514    108
       3002.45   7.511    151
       3000.49   7.506     44
       2996.71   7.496     65
       2996.22   7.495     66
       2995.49   7.493    143
       2994.88   7.492    112
       2994.15   7.490    136
       2992.19   7.485     32
       2919.44   7.303     50
       2918.34   7.300     84
       2916.75   7.296     34
       2911.26   7.283    172
       2909.80   7.279     95
       2905.03   7.267     46
       2903.57   7.263     98
       2903.08   7.262     86
       2901.49   7.258     24
       2888.31   7.225     42
       2886.97   7.222     81
       2885.63   7.218     51
       2881.84   7.209     31
       2879.52   7.203     81
       2877.32   7.198     25
       2873.66   7.189     19
       2872.32   7.185     32
       2871.10   7.182     18
       1247.69   3.121   1000
       1175.54   2.941      7
    

in CDCl3



KBr disk



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