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网站主页CAS数据库列表 2235-00-9更多图谱N-乙烯基己内酰胺(2235-00-9)质谱(MS)

N-乙烯基己内酰胺

产品名称 N-乙烯基己内酰胺

CAS号2235-00-9

分子式C8H13NO

分子量139.19

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  • Mass

    MS-IW-9664          
    1-vinylhexahydro-2-azepinone
    C8H13NO             (Mass of molecular ion:    139)
    

       Source Temperature: 220 °C
       Sample Temperature: 150 °C
       Reservoir, 75 eV
    

          15.0       2.3
          26.0       2.6
          27.0      20.9
          28.0      37.4
          29.0       7.7
          30.0       6.9
          38.0       1.0
          39.0      14.1
          40.0       4.0
          41.0      32.7
          42.0      16.6
          43.0      12.8
          44.0      37.6
          45.0       1.1
          51.0       1.0
          52.0       1.3
          53.0       3.5
          54.0      16.9
          55.0      42.3
          56.0     100.0
          57.0      19.7
          58.0       1.8
          67.0       6.5
          68.0      25.2
          69.0      12.8
          70.0      21.9
          71.0       1.5
          75.0       1.2
          77.0       1.0
          79.0       1.4
          80.0       2.5
          81.0       1.2
          82.0      34.7
          83.0      13.1
          84.0      12.4
          85.0       1.2
          94.0       1.0
          96.0      41.6
          97.0       4.3
         110.0      10.3
         111.0      13.0
         112.0       1.1
         138.0       5.1
         139.0      62.3
         140.0       6.7
    

400 MHz in CDCl3


  • 1H NMR 399.65 MHz
    C8H13NO 0.039 g : 0.5 ml CDCl3
    1-vinylhexahydro-2-azepinone
    ChemicalStructure
        Assign.     Shift(ppm)
    A 7.381 B 4.466 C 4.399 D 3.586 E 2.630 F 1.74 G 1.672

         Hz     ppm     Int.
    

       2963.38   7.413    613
       2954.11   7.390    633
       2947.27   7.373    642
       2937.87   7.349    634
       1793.71   4.487    619
       1792.49   4.484    641
       1777.59   4.447    601
       1776.37   4.444    643
       1763.80   4.412    728
       1762.58   4.409    690
       1754.52   4.389    729
       1753.30   4.386    656
       1437.87   3.597   1000
       1432.87   3.585    581
       1428.11   3.573    854
       1057.13   2.645    934
       1050.79   2.629    585
       1048.47   2.623    411
       1045.90   2.617    761
        717.41   1.795     78
        714.73   1.788    120
        711.80   1.781    195
        709.23   1.775    259
        704.11   1.762    515
        697.51   1.745    778
        696.17   1.742    872
        693.97   1.736    725
        688.60   1.723    510
        682.99   1.709    297
        680.30   1.702    257
        676.76   1.693    386
        671.64   1.680    474
        667.00   1.669    558
        661.87   1.656    368
        656.26   1.642    182
    

in CDCl3



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