-
MassMS-IW-7563 (R)-alpha-(2-pyrrolidinyl)benzhydryl alcohol C17H19NO (Mass of molecular ion: 253)
Source Temperature: 150 °C Sample Temperature: 120 °C Direct, 75 eV
18.0 1.1 28.0 3.5 41.0 2.7 43.0 4.5 51.0 1.9 68.0 3.0 69.0 1.8 70.0 100.0 71.0 6.5 77.0 8.7 78.0 1.0 105.0 10.8 152.0 1.3 165.0 2.6 167.0 1.9 176.0 1.1 181.0 1.4 182.0 4.2 183.0 1.7 206.0 2.0 234.0 6.6 235.0 6.9 236.0 1.2
400 MHz in CDCl3
-
1H NMR 399.65 MHz C17 H19 N O 0.041 g : 0.5 ml CDCl3 (R)-alpha-(2-pyrrolidinyl)benzhydryl alcohol 
Assign. Shift(ppm)
A *1 7.560 B *1 7.491 C *2 7.28 D *2 7.26 E *3 7.15 F *3 7.14 G 4.231 J *4 2.998 K *4 2.909 L 1.70 M 1.57
Hz ppm Int.3027.10 7.575 468 3025.76 7.572 570 3023.80 7.567 180 3019.53 7.556 336 3018.55 7.553 621 3017.46 7.551 592 3015.38 7.546 95 2999.51 7.506 487 2998.17 7.502 589 2996.22 7.498 184 2991.94 7.487 345 2990.97 7.484 649 2989.87 7.482 608 2987.92 7.477 106 2917.60 7.301 95 2915.89 7.297 355 2913.94 7.292 151 2908.45 7.278 947 2900.63 7.258 1000 2894.65 7.243 207 2893.07 7.240 429 2891.11 7.235 100 2866.94 7.174 155 2865.72 7.171 285 2864.38 7.168 201 2863.77 7.166 203 2862.43 7.163 299 2861.21 7.160 197 2860.11 7.157 170 2858.40 7.153 385 2857.06 7.149 233 2855.10 7.145 379 2853.27 7.140 143 2852.29 7.137 128 2851.07 7.134 181 2849.73 7.131 119 2849.12 7.130 120 2847.78 7.126 164 2846.56 7.123 94 1698.36 4.250 234 1690.67 4.231 422 1683.11 4.212 216 1195.56 2.992 159 1194.21 2.989 162 1189.09 2.976 146 1173.95 2.938 147 1166.75 2.920 320 1159.18 2.901 194 1157.47 2.897 226 693.12 1.735 139 685.91 1.717 203 684.08 1.712 190 682.01 1.707 133 679.57 1.701 220 676.88 1.694 198 674.56 1.688 183 672.00 1.682 145 667.36 1.670 179 655.76 1.641 153 648.32 1.623 145 629.27 1.575 204 621.83 1.556 194
in CDCl3
KBr disc
nujol mull
更多供应商
