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MassMS-NW-8867 p-chlorophenyl 2,3-epoxypropyl ether C9H9ClO2 (Mass of molecular ion: 184)
Source Temperature: 280 °C Sample Temperature: 140 °C Reservoir, 75 eV
15.0 1.1 26.0 1.5 27.0 17.6 28.0 2.0 29.0 48.2 30.0 1.2 31.0 37.6 37.0 1.2 38.0 3.8 39.0 8.3 41.0 2.6 43.0 4.2 49.0 1.2 50.0 5.7 51.0 3.9 53.0 1.3 55.0 1.8 57.0 57.1 58.0 2.1 61.0 1.6 62.0 3.5 63.0 11.6 64.0 6.8 65.0 15.5 66.0 1.2 73.0 10.1 74.0 3.4 75.0 16.5 76.0 2.8 77.0 5.7 85.0 1.7 89.0 1.4 91.0 6.3 92.0 2.2 93.0 2.6 99.0 13.2 100.0 7.8 101.0 4.8 102.0 2.8 111.0 20.9 112.0 2.0 113.0 12.9 114.0 1.1 115.0 2.1 119.0 3.9 125.0 5.6 127.0 4.9 128.0 100.0 129.0 7.8 130.0 32.4 131.0 2.2 141.0 23.5 142.0 2.0 143.0 7.8 153.0 1.0 154.0 12.2 155.0 2.0 156.0 4.1 184.0 71.5 185.0 7.2 186.0 23.4 187.0 2.3
400 MHz in CDCl3
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1H NMR 399.65 MHz C9 H9 Cl O2 0.039 g : 0.5 ml CDCl3 p-chlorophenyl 2,3-epoxypropyl ether 
Assign. Shift(ppm)
A 7.229 B 6.847 C *1 4.206 D *1 3.892 E 3.335 F 2.899 G 2.743
Hz ppm Int.2897.34 7.250 92 2893.92 7.242 971 2891.72 7.236 290 2889.53 7.231 40 2887.21 7.225 318 2884.89 7.219 1000 2881.47 7.210 105 2744.02 6.867 102 2740.60 6.858 973 2738.40 6.852 284 2733.89 6.841 278 2731.57 6.835 851 2728.15 6.827 83 1688.60 4.226 282 1685.55 4.218 284 1677.49 4.198 331 1674.56 4.191 334 1563.72 3.913 316 1557.98 3.899 331 1552.73 3.886 268 1546.88 3.871 281 1340.82 3.355 94 1338.01 3.348 170 1336.67 3.345 122 1335.08 3.341 203 1333.86 3.338 192 1332.28 3.334 180 1330.93 3.331 210 1329.35 3.327 114 1328.13 3.324 175 1325.20 3.316 98 1163.33 2.911 343 1159.18 2.901 385 1158.45 2.899 442 1154.30 2.889 382 1099.85 2.753 346 1097.17 2.746 346 1094.97 2.740 304 1092.29 2.734 294
in CDCl3
KBr disc
nujol mull
4880 A,200 M,liquid
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