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(R)-1-(4-硝基-苯基)乙基胺

产品名称 (R)-1-(4-硝基-苯基)乙基胺

CAS号22038-87-5

分子式C8H10N2O2

分子量166.18

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  • Mass

    MS-IW-3639          
    (R)-(-)-alpha-methyl-4-nitrobenzylamine hydrochloride
    C8H10N2O2 HCl       (Mass of molecular ion:    166)
    

       Source Temperature: 110 °C
       Sample Temperature:  90 °C
       Direct, 75 eV
    

          18.0       1.3
          28.0       2.5
          35.0       1.3
          36.0      13.0
          38.0       4.3
          39.0       1.3
          42.0       3.6
          43.0       4.6
          44.0       9.7
          50.0       2.4
          51.0       3.2
          52.0       1.4
          63.0       1.1
          65.0       1.1
          66.0       1.0
          74.0       1.0
          75.0       1.0
          76.0       1.8
          77.0       6.2
          78.0       3.7
          91.0       1.9
          93.0       3.9
         103.0       2.4
         104.0       9.0
         105.0      28.7
         106.0       2.5
         107.0       2.1
         118.0       1.6
         119.0       4.9
         121.0       2.0
         151.0     100.0
         152.0       8.5
         165.0       2.3
    

400 MHz in DMSO-d6


  • 1H NMR 399.65 MHz
    C8 H10 N2 O2 0.037 g : 0.5 ml DMSO-d6
    (R)-(-)-alpha-methyl-4-nitrobenzylamine hydrochloride
    ChemicalStructure
        Assign.     Shift(ppm)
    A 9.00 B 8.281 C 7.898 D 4.604 E 1.588

         Hz     ppm     Int.
    

       3598.33   9.004    491
       3316.80   8.300     96
       3314.21   8.293    689
       3312.38   8.289    309
       3307.34   8.276    260
       3305.36   8.271    828
       3163.15   7.915    112
       3160.86   7.910    700
       3153.84   7.892    237
       3152.01   7.887    657
       1850.28   4.630     72
       1843.41   4.613    237
       1836.70   4.596    241
       1829.83   4.579     74
        637.97   1.597    995
        631.26   1.580   1000
    

in DMSO-d6



KBr disc



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