硫代异烟酰胺

Mass

MS-NW-4781          
thioisonicotinamide
C6H6N2S             (Mass of molecular ion:    138)

   Source Temperature: 170 °C
   Sample Temperature: 110 °C
   Direct, 75 eV

      18.0       3.3
      26.0       2.5
      28.0       4.8
      32.0       1.3
      33.0       1.0
      34.0       1.9
      37.0       1.4
      38.0       1.7
      39.0       3.9
      45.0       2.2
      49.0       1.5
      50.0       8.7
      51.0      20.3
      52.0      13.9
      53.0       2.7
      59.0       1.0
      60.0      26.6
      62.0       1.5
      64.0       2.1
      66.0       1.1
      67.0       1.3
      69.0       3.2
      75.0       1.6
      76.0       3.8
      77.0       7.9
      78.0      18.2
      79.0      19.6
      80.0       1.3
      83.0       1.1
      84.0       1.2
      93.0       1.2
      95.0       1.0
     103.0       1.4
     104.0      14.5
     105.0      28.1
     106.0       2.6
     110.0       2.8
     111.0       2.7
     122.0      10.9
     137.0       4.8
     138.0     100.0
     139.0       8.6
     140.0       5.0

Parameter ppm Hz D(A) 8.94 D(B) 8.06 J(A,A') 0.4 J(A,B) 5.0 J(A,B') 0.8 J(A',B) 0.8 J(A',B') 5.0 J(B,B') 1.5 D(C) 10.4 BRUEGEL,W. Z.ELEKTROCHEM.(BER.BUNSENGES.PHYS.CHEM.) 66, 159 (1962) H(C):BROAD.

     Hz     ppm     Int.

   3120.01  10.400   1000
   2684.91   8.950    332
   2683.57   8.945    202
   2680.50   8.935    203
   2679.16   8.931    348
   2420.86   8.070    347
   2419.51   8.065    203
   2416.45   8.055    202
   2415.11   8.050    332