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网站主页CAS数据库列表 2170-09-4更多图谱N-甲基邻甲苯酰胺(2170-09-4)核磁图(13CNMR)

N-甲基邻甲苯酰胺

产品名称 N-甲基邻甲苯酰胺

CAS号2170-09-4

分子式C9H11NO

分子量149.19


  • Mass

    MS-IW-0862          
    N-methyl-o-toluamide
    C9H11NO             (Mass of molecular ion:    149)
    

       Source Temperature: 220 °C
       Sample Temperature: 150 °C
       Reservoir, 75 eV
    

          39.0       3.0
          41.0       1.0
          51.0       1.5
          58.0       1.6
          63.0       2.4
          65.0      12.1
          73.5       1.0
          77.0       1.1
          89.0       3.5
          90.0       4.6
          91.0      64.9
          92.0       5.2
         118.0      15.3
         119.0     100.0
         120.0       9.0
         134.0       5.1
         148.0      18.7
         149.0      68.2
         150.0       7.4
    

400 MHz in CDCl3


  • 1H NMR 399.65 MHz
    C9 H11 N O 0.039 g : 0.5 ml CDCl3
    N-methyl-o-toluamide
    ChemicalStructure
        Assign.     Shift(ppm)
    A 7.26 B 7.17 C 7.14 D 6.2 E 2.897 F 2.377 J(D,E)=4.9HZ CONFIRMED BY LAOCN PROGRAM

         Hz     ppm     Int.
    

       2912.84   7.289     56
       2911.38   7.285     91
       2909.67   7.281    231
       2907.96   7.277    131
       2904.30   7.268    158
       2901.86   7.262    168
       2900.39   7.258    175
       2897.71   7.251    147
       2896.24   7.247     68
       2869.38   7.180    167
       2864.87   7.169     40
       2861.08   7.159    117
       2860.35   7.158    144
       2852.54   7.138    119
       2851.68   7.136    123
       2844.85   7.119     53
       2844.24   7.117     51
       2469.85   6.181     30
       1160.28   2.904    965
       1155.40   2.892    941
        950.20   2.378   1000
    

in CDCl3



KBr disc



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