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网站主页CAS数据库列表 21378-21-2更多图谱3-甲基-2-环己烯-1-醇(21378-21-2)核磁图(13CNMR)

3-甲基-2-环己烯-1-醇

产品名称 3-甲基-2-环己烯-1-醇

CAS号21378-21-2

分子式C7H12O

分子量112.17

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  • Mass

    MS-NW-5616          
    3-methyl-2-cyclohexen-1-ol
    C7H12O              (Mass of molecular ion:    112)
    

       Source Temperature: 270 °C
       Sample Temperature: 190 °C
       Reservoir, 75 eV
    

          15.0       1.3
          17.0       1.7
          18.0       7.8
          26.0       1.2
          27.0      12.6
          28.0       2.7
          29.0       5.5
          31.0       2.1
          37.0       1.0
          38.0       2.6
          39.0      22.3
          40.0       4.7
          41.0      23.2
          42.0       2.7
          43.0      11.0
          44.0       1.5
          45.0       1.5
          50.0       3.0
          51.0       6.8
          52.0       3.0
          53.0       9.6
          54.0       4.1
          55.0      14.8
          56.0       6.7
          57.0       3.1
          58.0       1.1
          62.0       1.4
          63.0       2.8
          65.0       6.2
          66.0       5.3
          67.0       9.7
          68.0       2.0
          69.0      20.5
          70.0       2.0
          71.0       1.4
          77.0      26.4
          78.0       4.6
          79.0      65.2
          80.0       5.2
          81.0       2.4
          82.0       3.5
          83.0      19.5
          84.0      31.3
          85.0       2.2
          91.0      12.7
          92.0       2.1
          93.0      10.3
          94.0      28.9
          95.0       5.7
          97.0     100.0
          98.0       6.8
         110.0       1.2
         111.0       5.8
         112.0       9.5
    

400 MHz in CDCl3

90 MHz in CDCl3


  • 1H NMR 399.65 MHz
    C7 H12 O 0.05 ml : 0.5 ml CDCl3
    3-methyl-2-cyclohexen-1-ol
    ChemicalStructure
        Assign.     Shift(ppm)
    A 5.485 B 4.161 C 2.49 D 1.90 E 1.80 to 1.710 F 1.678 G 1.63 to 1.500

         Hz     ppm     Int.
    

       2195.80   5.495    101
       2194.21   5.491    172
       2192.63   5.487    207
       2190.92   5.483    199
       2189.33   5.479    156
       2187.74   5.475     80
       1661.87   4.159    116
        995.85   2.492    134
        785.64   1.966     40
        784.79   1.964     48
        783.81   1.962     50
        782.96   1.960     46
        782.10   1.957     38
        772.34   1.933     63
        771.61   1.931     63
        770.75   1.929     65
        769.90   1.927     69
        768.92   1.924     78
        768.07   1.922     98
        767.21   1.920    114
        766.36   1.918    118
        765.50   1.916    113
        762.82   1.909     67
        761.96   1.907     64
        761.11   1.905     66
        760.13   1.902     66
        759.40   1.901     64
        758.67   1.899     64
        757.81   1.897     68
        756.96   1.895     70
        755.98   1.892     70
        755.13   1.890     68
        754.03   1.887     68
        753.17   1.885     75
        752.32   1.883     85
        751.46   1.881     99
        750.61   1.879    108
        749.63   1.876    105
        748.78   1.874     96
        747.92   1.872     86
        746.95   1.870     78
        746.09   1.867     73
        745.24   1.865     65
        744.51   1.863     51
        733.89   1.837     44
        733.03   1.835     51
        732.18   1.833     52
        731.45   1.831     47
        730.47   1.828     38
        725.71   1.816     40
        724.85   1.814     46
        724.12   1.812     49
        718.99   1.800     41
        718.26   1.798     40
        715.58   1.791    110
        714.48   1.788    113
        711.79   1.782    151
        710.82   1.779    164
        707.89   1.772     66
        706.67   1.769    140
        705.81   1.767    151
        700.68   1.754    239
        696.41   1.743    153
        695.43   1.741    152
        691.04   1.730     56
        690.19   1.727     71
        687.38   1.720     57
        686.28   1.718     49
        685.55   1.716     43
        683.47   1.711     44
        682.13   1.707     49
        680.66   1.704     60
        679.93   1.702     63
        679.08   1.700     59
        677.98   1.697     63
        672.61   1.683    476
        671.75   1.681    778
        671.26   1.680    818
        670.41   1.678   1000
        669.43   1.676    726
        668.95   1.674    641
        667.97   1.672    371
        635.50   1.591     53
        635.13   1.590     52
        634.28   1.588     47
        630.98   1.579    124
        629.27   1.575    107
        627.69   1.571    165
        626.95   1.569    162
        626.10   1.567    163
        623.29   1.560    140
        621.70   1.556    147
        617.92   1.547    141
        614.62   1.538    145
        613.77   1.536    141
        611.57   1.531     72
    


  • 1H NMR 89.56 MHz
    C7 H12 O 0.04 ml : 0.5 ml CDCl3
    3-methyl-2-cyclohexen-1-ol
    ChemicalStructure
        Assign.     Shift(ppm)
    A 5.49 B 4.16 C 2.05 to 1.30 D 1.80 E 1.68

         Hz     ppm     Int.
    

        495.44   5.532     51
        494.19   5.518    106
        492.75   5.502    128
        490.63   5.479    124
        489.38   5.465    112
        489.25   5.463    112
        488.13   5.451     70
        378.75   4.230     32
        377.00   4.210     47
        375.56   4.194     66
        374.94   4.187     66
        374.06   4.177     79
        373.25   4.168     76
        372.63   4.161     81
        372.00   4.154     80
        370.31   4.135     74
        368.88   4.119     63
        367.00   4.098     40
        178.44   1.993     30
        175.56   1.961     75
        174.38   1.948     79
        173.38   1.936     89
        170.25   1.901    184
        167.25   1.868    223
        166.38   1.858    225
        165.44   1.848    249
        161.00   1.798    389
        157.19   1.756    155
        156.38   1.747    150
        154.75   1.728    226
        152.88   1.708    351
        151.50   1.692    792
        150.63   1.682   1000
        149.25   1.667    748
        145.44   1.624    229
        143.81   1.606    190
        141.06   1.576    122
        139.13   1.554     88
        137.63   1.537     92
        137.19   1.532     94
        136.56   1.525     88
        135.06   1.509     67
        132.69   1.482     57
        130.19   1.454     42
        128.13   1.431     30
    

in CDCl3



liquid film



4880 A,200 M,liquid