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MassMS-NW-9593 2-methylthiosemicarbazide C2H7N3S (Mass of molecular ion: 105)
Source Temperature: 190 °C Sample Temperature: 120 °C Direct, 75 eV
15.0 1.7 18.0 7.9 28.0 11.2 29.0 1.8 30.0 7.6 31.0 11.5 32.0 1.3 42.0 1.4 43.0 3.0 44.0 1.4 45.0 26.7 46.0 61.1 47.0 1.4 55.0 1.4 56.0 1.6 57.0 3.1 59.0 2.8 60.0 25.7 61.0 1.8 62.0 1.4 71.0 1.4 88.0 1.1 89.0 1.5 105.0 100.0 106.0 8.5 107.0 4.6
400 MHz in DMSO-d6
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1H NMR 399.65 MHz C2 H7 N3 S 0.040 g : 0.5 ml DMSO-d6 2-methylthiosemicarbazide 
Assign. Shift(ppm)
A *1 7.35 B *1 4.88 C 3.43 D 3.420
Hz ppm Int.2937.50 7.351 121 1950.93 4.882 198 1369.75 3.428 1000 1366.82 3.421 789
in DMSO-d6
KBr disc
nujol mull
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