3-硝基联苯

Mass

MS-KW-0498          
3-nitrobiphenyl
C12H9NO2            (Mass of molecular ion:    199)

   Source Temperature: 230 °C
   Sample Temperature: 150 °C
   Reservoir, 75 eV

      27.0       1.0
      39.0       2.4
      41.0       1.2
      43.0       1.5
      50.0       3.0
      51.0       5.8
      52.0       1.0
      56.0       1.0
      57.0       2.1
      62.0       1.5
      63.0       6.5
      65.0       1.2
      74.0       2.8
      75.0       4.9
      75.5       3.7
      76.0      18.6
      76.5       4.3
      77.0       6.4
      86.0       1.1
      87.0       1.3
      99.5       2.1
     101.0       1.8
     102.0       2.6
     115.0       3.7
     126.0       4.6
     127.0       7.2
     139.0       1.4
     141.0       8.0
     142.0       1.1
     150.0       4.9
     151.0      20.1
     152.0      80.8
     153.0      70.9
     154.0       9.1
     169.0       3.2
     199.0     100.0
     200.0      13.7
     201.0       1.3

Assign. Shift(ppm) A 8.420 B 8.166 C 7.881 D 7.58 E 7.55 to 7.44

     Hz     ppm     Int.

    756.50   8.447    272
    756.06   8.442    322
    754.25   8.422    625
    752.44   8.402    393
    752.06   8.398    404
    737.56   8.236    244
    736.38   8.223    286
    735.31   8.211    223
    734.06   8.197    219
    729.56   8.147    297
    728.31   8.133    358
    727.31   8.121    289
    726.06   8.107    302
    712.25   7.953    208
    711.00   7.939    258
    710.50   7.934    243
    709.25   7.920    233
    704.50   7.867    395
    703.25   7.853    374
    702.75   7.847    463
    701.50   7.833    336
    687.06   7.672    219
    686.13   7.662    501
    685.63   7.656    649
    683.25   7.629    311
    682.13   7.617    385
    680.69   7.601    268
    679.38   7.586    317
    678.44   7.576    962
    676.63   7.556   1000
    674.88   7.536    396
    674.06   7.527    414
    672.81   7.513    512
    671.00   7.493    747
    670.25   7.484    981
    668.56   7.465    560
    667.94   7.459    452
    666.31   7.440    485
    665.25   7.428    773
    663.06   7.404    815
    661.75   7.389    172