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网站主页CAS数据库列表 21087-29-6更多图谱肉桂基氯(21087-29-6)核磁图(1HNMR)

肉桂基氯

产品名称 肉桂基氯

CAS号21087-29-6

分子式C9H9Cl

分子量152.62

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  • Mass

    MS-NW-5818          
    trans-(3-chloro-1-propenyl)benzene
    C9H9Cl              (Mass of molecular ion:    152)
    

       Source Temperature: 260 °C
       Sample Temperature: 190 °C
       Reservoir, 75 eV
    

          27.0       1.1
          36.0       1.6
          38.0       1.0
          39.0       6.4
          50.0       2.6
          51.0       4.9
          52.0       1.1
          57.0       1.8
          57.5       5.1
          58.0       4.2
          62.0       1.8
          63.0       4.4
          65.0       3.3
          74.0       1.2
          75.0       1.2
          76.0       1.0
          77.0       2.1
          78.0       1.1
          89.0       3.5
          91.0      14.3
          92.0       1.2
         102.0       1.7
         115.0      33.2
         116.0      13.8
         117.0     100.0
         118.0      10.0
         152.0      19.9
         153.0       2.1
         154.0       6.5
    

90 MHz in CDCl3


  • 1H NMR 89.56 MHz
    C9 H9 Cl 0.04 ml : 0.5 ml CDCl3
    trans-(3-chloro-1-propenyl)benzene
    ChemicalStructure
        Assign.     Shift(ppm)
    A 7.54 to 7.08 B 6.600 C 6.302 D 4.202 J(B,C)=15.6HZ. J(C,D)=6.6HZ.

         Hz     ppm     Int.
    

        670.09   7.483     30
        669.49   7.476     33
        668.04   7.460     40
        666.85   7.446     32
        666.25   7.440     31
        665.05   7.426     53
        663.09   7.404    108
        662.23   7.395    160
        661.21   7.383    122
        660.10   7.371    113
        658.13   7.349    394
        656.16   7.327   1000
        654.80   7.312    971
        654.20   7.305    900
        653.09   7.293    383
        650.95   7.269    336
        649.41   7.252    226
        648.39   7.240     88
        646.85   7.223    141
        645.65   7.210     67
        645.23   7.205     69
        644.03   7.192     84
        642.66   7.176     37
        641.38   7.162     40
        603.02   6.734    118
        602.33   6.726    150
        586.69   6.551    422
        575.33   6.424    223
        568.66   6.350    342
        562.00   6.276    206
        559.69   6.250     58
        553.03   6.175    121
        546.36   6.101    100
        379.82   4.241    595
        379.05   4.233    623
        373.07   4.166    688
    

in CDCl3



liquid film