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MassMS-IW-9265 4-bromo-2-fluorophenol C6H4BrFO (Mass of molecular ion: 190)
Source Temperature: 210 °C Sample Temperature: 150 °C Reservoir, 75 eV
28.0 2.9 31.0 4.9 36.0 1.5 37.0 2.9 38.0 3.1 39.0 2.7 41.0 1.4 49.0 1.4 50.0 3.6 51.0 1.7 53.0 3.2 55.0 2.9 56.0 3.4 57.0 19.6 61.0 4.6 62.0 6.0 63.0 34.3 64.0 2.3 68.0 1.6 71.0 2.5 72.0 2.1 74.0 1.5 79.0 1.0 80.0 2.0 81.0 7.2 82.0 5.6 83.0 26.5 84.0 1.6 85.0 1.9 86.0 1.9 91.0 1.2 94.0 1.1 95.0 7.1 96.0 6.8 110.0 2.5 111.0 8.9 142.0 15.9 143.0 1.1 144.0 15.5 145.0 1.0 161.0 3.0 163.0 3.0 170.0 10.9 172.0 10.6 189.0 1.0 190.0 100.0 191.0 7.6 192.0 97.2 193.0 6.4
400 MHz in CDCl3
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1H NMR 399.65 MHz C6 H4 Br F O 0.05 ml : 0.5 ml CDCl3 4-bromo-2-fluorophenol 
Assign. Shift(ppm)
A 7.206 B 7.124 C 6.873 D 5.71
Hz ppm Int.2886.23 7.222 802 2883.91 7.217 854 2880.98 7.209 41 2876.22 7.197 768 2873.90 7.192 872 2871.22 7.185 42 2853.64 7.141 544 2852.17 7.137 552 2851.44 7.135 468 2849.98 7.132 424 2847.78 7.126 43 2844.97 7.119 594 2843.51 7.116 635 2842.77 7.114 569 2841.31 7.110 517 2838.01 7.102 33 2755.74 6.896 843 2751.10 6.884 38 2746.58 6.873 1000 2742.43 6.863 38 2737.79 6.851 727 2280.76 5.707 897
in CDCl3
liquid film
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