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MS-NW-2411 O-(p-nitrobenzyl)hydroxylamine hydrochloride C7H8N2O3 HCl (Mass of molecular ion: 168)
Source Temperature: 210 °C Sample Temperature: 140 °C Direct, 75 eV
16.0 1.9 17.0 2.1 18.0 10.0 27.0 1.8 28.0 3.4 29.0 2.3 30.0 34.4 32.0 2.1 35.0 4.4 36.0 33.7 37.0 1.3 38.0 11.0 39.0 6.7 40.0 1.4 50.0 10.5 51.0 14.7 52.0 5.2 62.0 2.3 63.0 8.1 64.0 4.8 65.0 2.5 74.0 3.5 75.0 4.6 76.0 6.0 77.0 13.2 78.0 50.6 79.0 4.1 89.0 21.2 90.0 25.8 91.0 3.1 92.0 2.0 104.0 2.4 105.0 3.0 106.0 24.6 107.0 3.8 120.0 2.8 136.0 100.0 137.0 9.9 150.0 5.2 151.0 5.2 153.0 1.0 168.0 1.6
400 MHz in DMSO-d6
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1H NMR 399.65 MHz C7 H8 N2 O3 0.039 g : 0.5 ml DMSO-d6 o-(p-nitrobenzyl)hydroxylamine hydrochloride Assign. Shift(ppm)
A 11.4 B 8.285 C 7.729 D 5.275
Hz ppm Int.
4571.84 11.440 31 3318.24 8.303 74 3315.86 8.297 559 3313.85 8.292 211 3309.09 8.280 198 3307.07 8.275 625 3304.69 8.269 99 3096.61 7.749 77 3094.23 7.743 506 3085.44 7.721 481 2108.80 5.277 1000
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