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MS-NW-6148 acenaphthylene C12H8 (Mass of molecular ion: 152)
Source Temperature: 260 °C Sample Temperature: 190 °C Reservoir, 75 eV
18.0 2.6 50.0 1.5 51.0 1.5 62.0 1.5 63.0 4.8 74.0 2.6 75.0 4.5 75.5 1.5 76.0 10.2 76.5 1.4 77.0 1.0 87.0 1.1 98.0 1.3 99.0 1.2 125.0 1.1 126.0 2.8 150.0 8.9 151.0 13.8 152.0 100.0 153.0 15.3 154.0 4.2
400 MHz in CDCl3
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1H NMR 399.65 MHz C12 H8 14.9 mg : 0.5 ml CDCl3 acenaphthylene Assign. Shift(ppm)
A 7.796 B 7.676 C 7.535 D 7.072
Hz ppm Int.
3120.24 7.808 245 3119.63 7.806 233 3111.94 7.787 277 3111.45 7.786 278 3071.66 7.686 240 3071.04 7.685 229 3064.70 7.669 314 3064.09 7.667 275 3018.07 7.552 273 3011.11 7.535 254 3009.77 7.532 283 3002.93 7.514 174 2826.54 7.073 1000
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