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四苯基碘化膦

产品名称 四苯基碘化膦

CAS号2065-67-0

分子式C24H20IP

分子量466.29

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  • Mass

    MS-IW-4961          
    tetraphenylphosphonium iodide
    C24H20IP            (Mass of molecular ion:    466)
    

       Source Temperature: 200 °C
       Sample Temperature: 320 °C
       Direct, 75 eV
    

          28.0       3.7
          51.0       1.4
          77.0       1.8
          78.0       2.7
         107.0       1.8
         108.0       4.8
         127.0       1.2
         128.0       1.9
         152.0       1.6
         154.0       1.0
         183.0       9.3
         184.0       2.3
         185.0       1.5
         261.0       2.2
         262.0       9.5
         263.0       1.9
         338.0       3.3
         339.0     100.0
         340.0      25.9
         341.0       3.5
         414.0       1.2
         415.0       8.3
         416.0       2.7
    

400 MHz in CDCl3


  • 1H NMR 399.65 MHz
    C24 H20 I P 0.039 g : 0.5 ml CDCl3
    tetraphenylphosphonium iodide
    ChemicalStructure
        Assign.     Shift(ppm)
    A 7.943 B 7.830 C 7.658

         Hz     ppm     Int.
    

       3185.55   7.971    121
       3184.33   7.968    227
       3183.23   7.966    200
       3182.37   7.963    237
       3181.15   7.960    151
       3178.83   7.955    184
       3176.76   7.949    610
       3174.93   7.945    615
       3172.97   7.940    210
       3170.53   7.934    258
       3169.31   7.931    440
       3168.33   7.928    362
       3167.24   7.926    420
       3166.02   7.922    220
       3141.60   7.861    146
       3139.89   7.857    559
       3138.31   7.853    353
       3136.35   7.848    598
       3134.77   7.844    361
       3131.96   7.837   1000
       3130.00   7.832    556
       3128.30   7.828    962
       3126.46   7.823    361
       3124.39   7.818    539
       3123.78   7.817    413
       3122.68   7.814    303
       3120.85   7.809    492
       3072.51   7.689    171
       3070.80   7.684    781
       3070.19   7.683    724
       3069.58   7.681    880
       3068.60   7.679    433
       3064.33   7.668    267
       3062.38   7.663    818
       3061.04   7.660    668
       3059.57   7.656    226
       3057.74   7.652    792
       3057.25   7.650    723
       3056.64   7.649    884
       3055.54   7.646    441
       3051.27   7.635    260
       3049.32   7.630    794
       3048.10   7.627    633
    

in CDCl3



KBr disc



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