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MS-NW-2102 N,N-dimethylacetoacetamide C6H11NO2 (Mass of molecular ion: 129)
Source Temperature: 250 °C Sample Temperature: 170 °C Reservoir, 75 eV
14.0 1.5 15.0 13.2 18.0 4.2 26.0 1.1 27.0 3.4 28.0 4.9 29.0 1.3 30.0 6.4 39.0 1.7 40.0 1.1 41.0 2.3 42.0 15.5 43.0 57.2 44.0 100.0 45.0 60.5 46.0 6.5 55.0 1.3 56.0 1.5 58.0 6.4 69.0 5.0 72.0 28.5 73.0 1.2 84.0 2.6 85.0 10.2 86.0 7.5 87.0 9.9 101.0 2.7 112.0 1.8 114.0 3.0 129.0 29.7 130.0 2.1
90 MHz in CDCl3
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1H NMR 89.56 MHz C6 H11 N O2 0.05 ml : 0.5 ml CDCl3 N,N-dimethylacetoacetamide Assign. Shift(ppm)
A 15. B 5.153 C 3.567 D 3.003 E 2.981 F 2.969 G 2.264 J 1.942
Hz ppm Int.
462.04 5.160 37 461.30 5.151 37 319.58 3.569 346 269.04 3.005 1000 267.09 2.983 586 265.99 2.970 768 202.88 2.266 699 196.78 2.198 21 174.32 1.947 122 173.71 1.940 124
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