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MassMS-NW-7297 2-phenyl-1-butanol C10H14O (Mass of molecular ion: 150)
Source Temperature: 200 °C Sample Temperature: 190 °C Reservoir, 75 eV
27.0 1.4 28.0 1.2 31.0 1.4 39.0 3.7 41.0 7.9 43.0 1.2 50.0 1.6 51.0 4.4 52.0 1.0 57.0 1.0 63.0 2.0 65.0 4.2 77.0 8.1 78.0 5.0 79.0 4.1 89.0 1.6 91.0 100.0 92.0 8.6 102.0 1.0 103.0 9.3 104.0 3.9 105.0 2.1 115.0 3.4 116.0 1.0 117.0 3.6 118.0 2.8 119.0 46.3 120.0 19.4 121.0 3.5 150.0 14.5 151.0 1.7
400 MHz in CDCl3
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1H NMR 399.65 MHz C10 H14 O 0.05 ml : 0.5 ml CDCl3 2-phenyl-1-butanol 
Assign. Shift(ppm)
A 7.297 B 7.21 C 7.17 D *1 3.68 E *1 3.66 F 2.636 G 1.87 J *2 1.730 K *2 1.542 L 0.811 J(D,E)=-10.9HZ J(D,F)=6.0HZ J(E,F)=7.8HZ
Hz ppm Int.2926.03 7.322 94 2925.05 7.320 150 2923.58 7.316 72 2919.80 7.306 102 2917.97 7.302 384 2911.87 7.287 124 2910.52 7.283 304 2908.57 7.278 79 2888.92 7.229 91 2887.57 7.226 185 2886.23 7.222 135 2882.32 7.213 68 2880.25 7.207 208 2878.05 7.202 83 2874.27 7.192 67 2872.80 7.189 176 2871.58 7.186 342 2870.12 7.182 383 2868.41 7.178 102 2864.99 7.169 135 2863.77 7.166 253 2863.28 7.165 281 2862.43 7.163 245 2860.35 7.158 46 1485.47 3.717 40 1479.49 3.702 51 1474.61 3.690 153 1468.02 3.674 292 1460.21 3.654 210 1457.15 3.647 67 1449.46 3.627 65 1067.87 2.673 31 1062.26 2.658 55 1060.30 2.654 42 1058.59 2.649 43 1056.52 2.644 43 1054.44 2.639 64 1052.98 2.635 68 1051.03 2.630 48 1048.95 2.625 42 1047.12 2.621 44 1045.29 2.616 60 1039.55 2.602 32 746.95 1.870 51 705.93 1.767 56 700.56 1.753 62 698.49 1.748 65 694.34 1.738 35 692.38 1.733 96 687.01 1.720 80 684.94 1.714 90 679.57 1.701 79 677.49 1.696 33 630.62 1.578 76 623.29 1.560 86 621.22 1.555 79 617.07 1.545 61 615.97 1.542 45 615.11 1.540 38 613.89 1.537 84 609.62 1.526 61 607.67 1.521 60 606.57 1.518 39 600.22 1.502 56 331.54 0.830 524 324.10 0.811 1000 316.77 0.793 519
in CDCl3
liquid film
4880 A,200 M,liquid
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