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网站主页CAS数据库列表 20279-21-4更多图谱1,2,3,10B-四氢荧蒽(20279-21-4)质谱(MS)

1,2,3,10B-四氢荧蒽

产品名称 1,2,3,10B-四氢荧蒽

CAS号20279-21-4

分子式C16H14

分子量206.28

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  • Mass

    MS-NW-5995          
    1,2,3,10b-tetrahydrofluoranthene
    C16H14              (Mass of molecular ion:    206)
    

       Source Temperature: 270 °C
       Sample Temperature: 190 °C
       Reservoir, 75 eV
    

          39.0       1.1
          51.0       1.5
          63.0       2.9
          74.0       1.6
          75.0       2.9
          76.0      11.3
          76.5       1.6
          77.0       1.2
          81.5       1.2
          82.5       2.4
          87.0       2.1
          88.0       6.9
          88.5       1.4
          89.0      15.7
          89.5       2.7
          94.0       1.2
          94.5       3.8
          95.0       1.8
          99.0       1.1
         100.0       3.7
         100.5       1.5
         101.0       7.6
         101.5       2.3
         102.0       2.5
         103.0       3.4
         126.0       1.1
         127.0       1.0
         128.0       1.0
         139.0       1.3
         150.0       2.4
         151.0       4.2
         152.0       5.7
         153.0       1.1
         163.0       2.2
         164.0       1.1
         165.0       6.7
         166.0       1.3
         174.0       1.1
         175.0       1.4
         176.0       7.8
         177.0       5.7
         178.0     100.0
         179.0      16.7
         180.0       1.5
         189.0       6.4
         190.0       5.0
         191.0       4.5
         200.0       3.6
         201.0       3.1
         202.0      14.7
         203.0      13.0
         204.0       6.7
         205.0      18.8
         206.0      62.3
         207.0      11.1
         208.0       1.0
    

400 MHz in CDCl3


  • 1H NMR 399.65 MHz
    C16 H14 0.040 g : 0.5 ml CDCl3
    1,2,3,10b-tetrahydrofluoranthene
    ChemicalStructure
        Assign.     Shift(ppm)
    A 7.757 B 7.55 C 7.53 D 7.292 E 7.287 F 7.255 G 7.059 J 3.652 K *1 3.043 L *1 2.766 M *2 2.561 N *3 2.12 P *3 2.10 S *2 1.218 ASSIGNED BY H-H AND C-H COSY

         Hz     ppm     Int.
    

       3093.99   7.742    678
       3087.40   7.726    595
       3086.55   7.724    770
       3009.77   7.532    685
       3009.16   7.530    666
       3005.49   7.521    400
       3004.52   7.518    708
       3003.42   7.516    848
       3002.44   7.513   1000
       2998.17   7.502    424
       2997.07   7.500    719
       2996.34   7.498    678
       2995.24   7.495    348
       2939.45   7.356    258
       2938.35   7.353    324
       2937.50   7.351    247
       2932.01   7.337    616
       2931.15   7.335    739
       2930.05   7.332    542
       2924.56   7.318    421
       2923.71   7.316    481
       2922.61   7.313    351
       2912.96   7.289    481
       2912.23   7.287    457
       2908.94   7.279    669
       2907.71   7.276    690
       2905.52   7.271    933
       2904.79   7.269    895
       2901.61   7.261    940
       2900.39   7.258    904
       2897.95   7.252    504
       2897.22   7.250    475
       2894.17   7.242    383
       2892.94   7.239    357
       2814.82   7.044    767
       2813.96   7.042    737
       2807.37   7.025    663
       2806.52   7.023    627
       1454.35   3.640    262
       1449.34   3.627    274
       1442.14   3.609    278
       1437.26   3.597    279
       1217.77   3.048    133
       1214.36   3.039    136
       1211.06   3.031    155
       1210.21   3.029    151
       1207.03   3.021    143
       1200.56   3.005    185
       1196.90   2.995    185
       1193.73   2.987    210
       1193.12   2.986    207
       1189.94   2.978    198
       1108.28   2.774    165
       1107.91   2.773    164
       1099.49   2.752    315
       1091.06   2.731    303
       1082.28   2.709    249
       1073.85   2.687    144
       1020.87   2.555    148
       1016.48   2.544    255
       1012.33   2.534    251
       1011.35   2.531    226
       1008.67   2.524    220
       1007.93   2.523    219
       1004.52   2.514    291
       1000.73   2.505    248
        999.76   2.502    270
        995.61   2.492    173
        857.54   2.146    253
        856.81   2.144    223
        853.76   2.137    362
        852.54   2.134    259
        851.44   2.131    271
        849.73   2.127    464
        847.90   2.122    491
        845.70   2.117    518
        844.60   2.114    307
        843.51   2.111    405
        841.92   2.107    363
        840.09   2.103    364
        838.75   2.099    244
        836.67   2.094    330
        834.35   2.088    186
        832.64   2.084    188
        829.59   2.076    156
        825.07   2.065    162
        493.04   1.234    171
        487.92   1.221    115
        487.18   1.220    105
        482.06   1.207    272
        480.96   1.204    333
        475.83   1.191    248
        474.85   1.189    199
        469.97   1.176    405
        468.75   1.173    196
        464.23   1.162    318
        457.89   1.146    189
        452.03   1.132    142
    

in CDCl3



KBr disc