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网站主页CAS数据库列表 2008-75-5更多图谱1-(2-氯乙基)哌啶盐酸盐(2008-75-5)质谱(MS)

1-(2-氯乙基)哌啶盐酸盐

产品名称 1-(2-氯乙基)哌啶盐酸盐

CAS号2008-75-5

分子式C7H15Cl2N

分子量184.11

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  • Mass

    MS-NW-7039          
    N-(2-chloroethyl)piperidine hydrochloride
    C7H14ClN HCl        (Mass of molecular ion:    147)
    

       Source Temperature: 170 °C
       Sample Temperature: 120 °C
       Direct, 75 eV
    

          15.0       2.2
          18.0       2.1
          26.0       1.0
          27.0       9.4
          28.0       6.7
          29.0       3.4
          30.0       3.5
          35.0       2.6
          36.0      16.1
          38.0       5.2
          39.0       3.7
          41.0      12.6
          42.0      19.6
          43.0       2.1
          44.0       6.5
          53.0       1.2
          54.0       2.3
          55.0      12.5
          56.0       3.9
          57.0       1.4
          63.0       2.9
          65.0       1.0
          69.0       4.1
          70.0       4.8
          83.0       1.0
          84.0       1.1
          96.0       1.7
          98.0     100.0
          99.0       6.9
         118.0       1.7
         146.0       2.6
         147.0       4.8
         148.0       1.2
         149.0       1.6
    

400 MHz in CDCl3


  • 1H NMR 399.65 MHz
    C7 H14 Cl N 0.039 g : 0.5 ml CDCl3
    N-(2-chloroethyl)piperidine hydrochloride
    ChemicalStructure
        Assign.     Shift(ppm)
    A 12.4 B 4.114 C 3.596 D 3.43 E 2.946 F 2.236 G 1.89 J 1.499

         Hz     ppm     Int.
    

       4951.72  12.391     36
       1651.25   4.132    516
       1644.47   4.115   1000
       1637.87   4.099    575
       1443.54   3.613    157
       1437.49   3.597     80
       1431.45   3.582    176
       1379.43   3.452    172
       1374.30   3.439    222
       1372.83   3.436    332
       1367.70   3.423    335
       1366.24   3.419    217
       1360.93   3.406    165
       1196.81   2.995     58
       1194.25   2.989     63
       1184.72   2.965    161
       1181.97   2.958    129
       1178.68   2.950     45
       1175.20   2.941    130
       1172.63   2.935    165
       1163.11   2.911     68
       1161.46   2.907     58
       1160.36   2.904     63
        915.28   2.291     46
        911.44   2.281     36
        903.74   2.262    105
        902.64   2.259    110
        900.26   2.253    112
        898.80   2.249    100
        894.95   2.240     45
        891.47   2.231    108
        889.82   2.227    112
        887.62   2.221    126
        882.86   2.210     47
        880.85   2.205     35
        880.30   2.203     36
        878.83   2.199     47
        877.55   2.196     40
        875.17   2.190     58
        872.06   2.183     35
        871.69   2.182     35
        760.51   1.903    246
        758.86   1.899    241
        749.15   1.875    228
        747.14   1.870    227
        612.69   1.534     30
        606.28   1.518     51
        605.00   1.514     60
        603.35   1.510     65
        600.24   1.502     65
        594.01   1.487     59
        590.90   1.479     60
        589.25   1.475     52
        587.96   1.472     46
    

in CDCl3



KBr disc



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