6-溴-2-羟基于-甲氧基苯甲醛

Mass

MS-IW-3606          
6-bromo-2-hydroxy-3-methoxybenzaldehyde
C8H7BrO3            (Mass of molecular ion:    230)

   Source Temperature: 210 °C
   Sample Temperature: 160 °C
   Reservoir, 75 eV

      15.0       1.9
      26.0       1.8
      27.0       1.5
      28.0       3.4
      29.0       5.8
      31.0       1.2
      37.0       3.7
      38.0       4.0
      39.0       4.7
      40.0       3.0
      41.0       1.3
      43.0       1.5
      45.0       7.3
      49.0       4.5
      50.0      14.7
      51.0      29.2
      52.0      13.0
      53.0      10.1
      54.0       6.4
      55.0       2.1
      61.0       5.7
      62.0       9.7
      63.0      13.0
      64.0       3.4
      65.0       6.1
      66.0       2.9
      74.0       2.9
      75.0       3.2
      77.0       7.8
      78.0       5.0
      79.0      24.9
      80.0      12.3
      82.0       1.2
      90.0       2.1
      91.0       1.9
      92.0       3.4
      93.0       2.1
      94.0       4.6
      95.0       1.8
     105.0       8.7
     106.0       2.8
     107.0      41.8
     108.0      20.8
     109.0       1.7
     117.0       1.3
     119.0       1.6
     121.0       1.5
     122.0       3.8
     123.0       1.9
     131.0       4.3
     133.0       5.1
     136.0       1.0
     143.0       2.2
     145.0       1.8
     151.0       2.0
     154.0       4.4
     156.0       4.6
     157.0       1.8
     158.0       1.5
     159.0       7.8
     160.0       1.5
     161.0       6.8
     170.0       2.1
     172.0       2.3
     173.0       1.1
     182.0       1.2
     183.0       1.6
     184.0      40.6
     185.0       5.6
     186.0      41.3
     187.0      33.9
     188.0       4.8
     189.0      29.6
     190.0       2.2
     198.0       3.9
     199.0       5.5
     200.0      10.8
     201.0      11.8
     202.0       8.0
     203.0       7.2
     204.0       1.0
     211.0       1.9
     212.0       1.4
     213.0       2.3
     214.0       6.4
     215.0       8.6
     216.0       5.7
     217.0       7.8
     229.0      17.0
     230.0     100.0
     231.0      25.1
     232.0      98.1
     233.0       9.0

Assign. Shift(ppm) A 12.3 B 10.284 C 7.084 D 6.916 E 3.898 J(A,D)=0.8HZ

     Hz     ppm     Int.

   4907.03  12.279    272
   4906.30  12.277    291
   4110.07  10.285    489
   2836.15   7.097    203
   2827.54   7.076    258
   2768.01   6.927    150
   2759.40   6.905    118
   1558.01   3.899   1000