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MassMS-IW-9553 p-cyclohexylbenzoic acid C13H16O2 (Mass of molecular ion: 204)
Source Temperature: 170 °C Sample Temperature: 120 °C Direct, 75 eV
18.0 1.8 27.0 3.6 28.0 1.9 29.0 2.9 39.0 6.5 41.0 11.9 45.0 1.0 50.0 1.5 51.0 4.5 52.0 1.1 53.0 2.8 54.0 2.7 55.0 4.7 63.0 2.7 64.0 1.2 65.0 3.5 67.0 8.0 68.0 1.2 69.0 6.7 75.0 1.3 76.0 1.6 77.0 11.1 78.0 2.3 79.0 3.1 81.0 5.7 82.0 7.5 83.0 1.0 89.0 2.5 90.0 1.9 91.0 32.8 92.0 6.1 99.0 5.3 102.0 2.3 103.0 7.3 104.0 2.5 105.0 4.2 107.0 5.5 115.0 12.9 116.0 4.2 117.0 36.5 118.0 5.2 119.0 1.0 123.0 8.1 127.0 1.4 128.0 3.0 129.0 4.0 130.0 1.1 131.0 19.5 132.0 2.2 135.0 18.4 136.0 10.7 137.0 1.2 143.0 1.0 145.0 1.7 148.0 100.0 149.0 11.2 150.0 1.1 157.0 1.1 159.0 34.3 160.0 5.0 161.0 5.6 162.0 3.7 168.0 2.0 175.0 1.5 186.0 2.6 187.0 2.1 203.0 1.0 204.0 68.0 205.0 9.9
400 MHz in DMSO-d6
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1H NMR 399.65 MHz C13 H16 O2 0.041 g : 0.5 ml DMSO-d6 p-cyclohexylbenzoic acid 
Assign. Shift(ppm)
A 12.8 B 7.884 C 7.335 D 2.56 E 1.78 F 1.702 G 1.38 J 1.238
Hz ppm Int.3155.23 7.895 927 3153.58 7.891 359 3148.63 7.879 367 3146.98 7.875 1000 2935.79 7.346 860 2931.40 7.335 98 2927.55 7.326 804 1034.71 2.590 73 1034.16 2.588 74 1033.79 2.587 74 1033.43 2.586 76 1032.69 2.584 79 1032.33 2.584 79 1030.13 2.578 64 1029.58 2.577 63 1029.21 2.576 64 1023.90 2.562 142 1021.34 2.556 126 1017.12 2.546 69 1013.28 2.536 100 1012.91 2.535 100 1011.81 2.532 104 1011.26 2.531 104 1010.35 2.529 103 1009.61 2.527 101 1009.25 2.526 100 718.01 1.797 508 717.28 1.795 505 711.42 1.781 354 706.66 1.769 555 687.61 1.721 131 685.96 1.717 143 685.59 1.716 142 679.73 1.701 69 677.72 1.696 94 674.97 1.689 133 674.60 1.688 133 673.69 1.686 141 673.32 1.685 142 580.27 1.452 68 568.00 1.422 216 558.47 1.398 534 549.68 1.376 433 548.22 1.372 406 542.72 1.358 90 539.79 1.351 163 537.59 1.346 205 527.15 1.320 62 524.96 1.314 77 524.59 1.313 77 509.20 1.275 61 496.93 1.244 108 484.66 1.213 84
in DMSO-d6
KBr disc
nujol mull
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