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MassMS-NW-8964 2,6-dichloroanisole C7H6Cl2O (Mass of molecular ion: 176)
Source Temperature: 260 °C Sample Temperature: 150 °C Reservoir, 75 eV
37.0 2.1 38.0 1.9 39.0 1.0 49.0 1.6 50.0 3.4 51.0 2.4 53.0 1.8 61.0 3.5 62.0 6.7 63.0 16.3 72.0 2.9 73.0 13.7 74.0 8.0 75.0 15.1 76.0 1.7 77.0 3.3 83.0 2.8 84.0 3.2 85.0 3.6 86.0 1.2 87.0 1.1 97.0 5.1 98.0 3.5 99.0 2.0 100.0 1.1 107.0 3.2 109.0 7.5 110.0 2.3 111.0 7.9 112.0 1.7 113.0 4.3 126.0 3.6 128.0 1.2 133.0 58.1 134.0 3.5 135.0 37.7 136.0 2.1 137.0 6.1 141.0 1.2 145.0 3.0 147.0 2.4 161.0 77.6 162.0 5.5 163.0 50.2 164.0 3.5 165.0 8.2 176.0 100.0 177.0 8.0 178.0 64.5 179.0 5.1 180.0 10.5
90 MHz in CDCl3
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1H NMR 89.56 MHz C7 H6 Cl2 O 0.04 ml : 0.5 ml CDCl3 2,6-dichloroanisole 
Assign. Shift(ppm)
A 7.27 B 6.97 C 3.90
Hz ppm Int.656.69 7.333 118 655.06 7.315 133 648.25 7.239 225 647.63 7.232 213 630.94 7.045 129 624.19 6.970 82 621.81 6.943 58 615.06 6.868 45 349.06 3.898 1000
in CDCl3
liquid film
4880 A,200 M,liquid
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