2,3-二氯茴香醚

Mass

MS-NW-6549          
2,3-dichloroanisole
C7H6Cl2O            (Mass of molecular ion:    176)

   Source Temperature: 260 °C
   Sample Temperature: 190 °C
   Reservoir, 75 eV

      15.0       2.8
      28.0       1.3
      29.0       1.4
      36.0       1.5
      37.0       4.1
      38.0       1.8
      39.0       2.3
      48.0       1.0
      49.0       2.2
      50.0       4.1
      51.0       2.4
      61.0       3.7
      62.0       6.3
      63.0      16.2
      64.0       1.0
      72.0       4.7
      73.0       8.3
      74.0       7.0
      75.0       9.4
      76.0       2.4
      77.0       5.9
      83.0       2.5
      84.0       3.0
      85.0       2.4
      86.0       1.2
      87.0       1.2
      97.0       4.9
      98.0       3.9
      99.0       1.9
     100.0       1.2
     107.0       4.4
     109.0       6.3
     110.0       2.3
     111.0       8.8
     112.0       2.6
     113.0       5.5
     115.0       1.3
     126.0       5.3
     128.0       1.9
     133.0      51.1
     134.0       3.4
     135.0      33.0
     136.0       2.0
     137.0       5.5
     141.0       2.7
     145.0       2.9
     146.0      13.7
     147.0       4.0
     148.0       8.9
     149.0       1.7
     150.0       1.6
     161.0      33.5
     162.0       2.6
     163.0      21.3
     164.0       1.6
     165.0       3.6
     176.0     100.0
     177.0       8.4
     178.0      64.4
     179.0       5.4
     180.0      10.7
     181.0       1.0

Assign. Shift(ppm) A 7.13 B 7.06 C 6.828 D 3.893 J(A,B)=8.1HZ. J(A,C)=7.0HZ. J(B,C)=2.7HZ.

     Hz     ppm     Int.

    649.19   7.249     33
    642.13   7.170     27
    641.13   7.159    127
    635.50   7.096    158
    634.06   7.080    248
    632.81   7.066    250
    627.44   7.006     65
    615.31   6.871     93
    612.63   6.841     66
    608.31   6.793     51
    605.56   6.762     46
    348.69   3.894   1000