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网站主页CAS数据库列表 1983-26-2更多图谱氯甲基膦酸二氯(1983-26-2)核磁图(13CNMR)

氯甲基膦酸二氯

产品名称 氯甲基膦酸二氯

CAS号1983-26-2

分子式CH2Cl3OP

分子量167.36


  • Mass

    MS-NW-8558          
    (chloromethyl)phosphonic dichloride
    CH2Cl3OP            (Mass of molecular ion:    166)
    

       Source Temperature: 260 °C
       Sample Temperature: 140 °C
       Reservoir, 75 eV
    

          29.0       2.4
          31.0       2.0
          35.0       3.0
          36.0       3.9
          38.0       1.3
          44.0       2.3
          45.0       1.4
          47.0      26.6
          48.0       4.0
          49.0     100.0
          50.0       2.4
          51.0      31.5
          66.0       6.5
          67.0       1.4
          68.0       2.5
          77.0       1.0
          79.0       1.0
          82.0       2.5
          83.0       6.6
          85.0       2.6
         101.0       8.3
         103.0       5.8
         105.0       1.1
         117.0      16.5
         119.0      10.8
         121.0       1.8
         130.0       4.3
         131.0       8.2
         132.0       3.0
         133.0       5.3
         136.0      16.3
         138.0      15.6
         140.0       5.0
         159.0       1.0
         166.0      12.5
         168.0      11.8
         170.0       3.9
    

90 MHz in CDCl3


  • 1H NMR 89.56 MHz
    C H2 Cl3 O P 0.05 ml : 0.5 ml CDCl3
    (chloromethyl)phosphonic dichloride
    ChemicalStructure
        Assign.     Shift(ppm)
    A 4.227 J(A,P-31)=6.1HZ

         Hz     ppm     Int.
    

        381.69   4.262   1000
        379.81   4.241     64
        378.88   4.231     59
        375.63   4.195    996
        372.88   4.164     45
    

in CDCl3



liquid film