苝

产品名称苝

CAS号198-55-0

分子式C20H12

分子量252.31

¹³CNMR

Mass

MS-NW-0115          
perylene
C20H12              (Mass of molecular ion:    252)

   Source Temperature: 220 °C
   Sample Temperature:   0 °C
   Direct, 75 eV

      18.0       2.4
      28.0       3.4
      32.0       1.4
     112.0       3.0
     112.5       1.0
     113.0       3.1
     124.0       4.1
     124.5       2.6
     125.0      10.7
     125.5       2.8
     126.0      13.8
     126.5       3.0
     224.0       1.6
     226.0       1.2
     248.0       3.4
     249.0       2.8
     250.0      18.1
     251.0       6.4
     252.0     100.0
     253.0      22.1
     254.0       2.3

400 MHz in CDCl3

90 MHz in CDCl3

¹H NMR	399.65 MHz
C₂₀ H₁₂	saturated in CDCl₃
perylene

    Assign.     Shift(ppm)

      A             8.188
      B             7.678
      C             7.479
     
     J(A,C)=J(B,C)=7.6HZ.

     Hz     ppm     Int.

   3282.10   8.213     27
   3276.37   8.199    691
   3268.68   8.179    749
   3260.74   8.159     41
   3258.54   8.154     30
   3257.93   8.152     28
   3257.69   8.152     28
   3256.96   8.150     28
   3256.47   8.149     28
   3255.62   8.147     27
   3080.08   7.707     26
   3072.75   7.689    638
   3064.82   7.669    784
   3056.15   7.648     34
   3055.18   7.645     29
   3054.08   7.642     26
   3000.37   7.508     42
   2996.22   7.498    689
   2988.65   7.479   1000
   2980.71   7.459    549

¹H NMR	89.56 MHz
C₂₀ H₁₂	0.017 g : 0.5 ml CDCl₃
perylene

    Assign.     Shift(ppm)

      A             8.179
      B             7.662
      C             7.478
     
     400MHZ : HSP-40-299

     Hz     ppm     Int.

    737.19   8.232    545
    735.81   8.216    530
    730.00   8.151    640
    728.63   8.136    693
    692.56   7.733    320
    691.13   7.717    413
    689.25   7.696     71
    684.38   7.642    883
    683.00   7.627    783
    681.00   7.604     69
    677.69   7.567     59
    675.56   7.544   1000
    668.31   7.463    858
    667.38   7.452    501
    660.19   7.372    345

in CDCl3

KBr disc

nujol mull

CATION RADICAL

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