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2,5-二氟苯乙酮

产品名称 2,5-二氟苯乙酮

CAS号1979-36-8

分子式C8H6F2O

分子量156.13

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  • Mass

    MS-IW-9015          
    2',5'-difluoroacetophenone
    C8H6F2O             (Mass of molecular ion:    156)
    

       Source Temperature: 200 °C
       Sample Temperature: 150 °C
       Reservoir, 75 eV
    

          15.0       1.9
          31.0       1.4
          42.0       1.5
          43.0      25.2
          50.0       2.1
          51.0       1.0
          57.0       2.7
          61.0       1.3
          62.0       2.8
          63.0      14.0
          68.0       1.7
          69.0       1.2
          70.5       1.8
          74.0       1.7
          75.0       1.7
          81.0       2.0
          93.0       1.9
          94.0       1.3
         101.0       1.1
         107.0       1.2
         112.0       1.5
         113.0      40.5
         114.0       5.5
         127.0       1.8
         141.0     100.0
         142.0       7.8
         156.0      36.9
         157.0       3.4
    

400 MHz in CDCl3


  • 1H NMR 399.65 MHz
    C8 H6 F2 O 0.05 ml : 0.5 ml CDCl3
    2',5'-difluoroacetophenone
    ChemicalStructure
        Assign.     Shift(ppm)
    A 7.536 B 7.220 C 7.139 D 2.643

         Hz     ppm     Int.
    

       3020.75   7.559     82
       3020.39   7.558     83
       3017.46   7.551     91
       3015.26   7.545     90
       3014.89   7.544     90
       3011.72   7.536    157
       3008.54   7.528     90
       3006.59   7.524     87
       3006.23   7.523     88
       3003.30   7.515     87
       3002.93   7.514     86
       2898.19   7.252     50
       2894.90   7.244     59
       2894.41   7.243     67
       2891.11   7.235     97
       2889.16   7.230     90
       2887.82   7.226     67
       2887.33   7.225     74
       2885.86   7.221    104
       2885.38   7.220    106
       2884.03   7.217     64
       2882.08   7.212    149
       2878.78   7.204     97
       2878.30   7.203    100
       2875.00   7.194     76
       2863.65   7.166    105
       2859.74   7.156    106
       2859.38   7.155    107
       2854.00   7.142    120
       2853.64   7.141    114
       2849.85   7.131    120
       2849.49   7.130    115
       2844.97   7.119     67
       2844.60   7.118     68
       2840.82   7.109     64
       2840.45   7.108     64
       1058.84   2.650   1000
       1053.71   2.637    966
    

in CDCl3



liquid film