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MS-NW-7476 2-bromo-N,N-dimethylbenzylamine C9H12BrN (Mass of molecular ion: 213)
Source Temperature: 240 °C Sample Temperature: 170 °C Reservoir, 75 eV
15.0 2.2 28.0 1.2 30.0 1.9 39.0 2.4 41.0 1.0 42.0 11.3 43.0 2.6 44.0 4.8 50.0 1.3 51.0 1.7 57.0 3.4 58.0 100.0 59.0 3.8 62.0 1.0 63.0 3.4 64.0 1.2 65.0 2.2 65.5 2.7 66.5 1.1 89.0 5.8 90.0 6.4 91.0 6.6 132.0 3.5 134.0 1.4 169.0 8.6 171.0 8.4 212.0 6.5 213.0 13.0 214.0 7.7 215.0 12.6 216.0 1.4
90 MHz in CDCl3
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1H NMR 89.56 MHz C9 H12 Br N 0.05 ml : 0.5 ml CDCl3 2-bromo-N,N-dimethylbenzylamine Assign. Shift(ppm)
A 7.51 B 7.39 C 7.20 D 7.04 E 3.512 F 2.278
Hz ppm Int.
677.50 7.565 34 676.00 7.549 33 670.00 7.482 70 668.25 7.462 74 662.94 7.403 45 662.44 7.397 46 660.75 7.378 54 656.19 7.327 29 654.69 7.311 31 649.06 7.248 57 647.56 7.231 49 641.75 7.166 34 639.31 7.139 46 637.06 7.114 38 631.75 7.054 35 629.69 7.031 32 314.56 3.513 231 204.13 2.280 1000
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