-
MassMS-NW-8611 o-bromophenyl methyl sulfide C7H7BrS (Mass of molecular ion: 202)
Source Temperature: 260 °C Sample Temperature: 140 °C Reservoir, 75 eV
37.0 1.8 38.0 3.3 39.0 4.9 43.0 1.0 45.0 27.7 46.0 3.8 47.0 4.7 49.0 1.5 50.0 13.1 51.0 9.0 54.0 1.2 57.0 1.1 58.0 4.3 60.0 1.8 61.0 2.3 62.0 3.4 63.0 10.1 64.0 1.7 65.0 1.0 69.0 18.0 70.0 1.2 71.0 1.4 73.0 1.5 74.0 7.3 75.0 8.9 76.0 6.5 77.0 18.1 78.0 5.3 79.0 5.0 81.0 4.3 82.0 8.4 89.0 1.6 90.0 2.4 91.0 1.7 93.0 1.4 102.0 1.0 106.0 1.0 107.0 2.8 108.0 67.0 109.0 5.4 110.0 3.1 121.0 10.4 122.0 13.4 123.0 11.9 124.0 1.9 156.0 8.2 157.0 1.4 158.0 8.1 169.0 17.4 170.0 1.3 171.0 17.0 172.0 1.3 187.0 10.1 188.0 1.2 189.0 10.4 201.0 2.0 202.0 97.8 203.0 10.1 204.0 100.0 205.0 8.5 206.0 4.6
90 MHz in CDCl3
-
1H NMR 89.56 MHz C7 H7 Br S 0.05 ml : 0.5 ml CDCl3 o-bromophenyl methyl sulfide 
Assign. Shift(ppm)
A 7.476 B 7.24 C 7.08 D 6.97 E 2.419 B,C AND D WERE CONFIRMED BY LAOCN PROGRAM.
Hz ppm Int.674.56 7.532 67 673.56 7.521 79 667.00 7.448 89 665.81 7.435 110 658.94 7.358 30 657.50 7.342 30 652.13 7.282 49 650.88 7.268 74 649.50 7.253 69 644.13 7.193 120 642.63 7.176 102 638.38 7.128 82 636.44 7.107 133 630.38 7.039 146 628.31 7.016 90 623.50 6.962 62 622.69 6.953 78 621.50 6.940 57 620.69 6.931 56 615.81 6.876 41 613.81 6.854 34 216.75 2.421 1000
in CDCl3
liquid film
更多供应商
