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2,4-二甲基-1-庚烯

产品名称 2,4-二甲基-1-庚烯

CAS号19549-87-2

分子式C9H18

分子量126.24

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  • Mass

    MS-NW-3198          
    2,4-dimethyl-1-heptene
    C9H18               (Mass of molecular ion:    126)
    

       Source Temperature: 300 °C
       Sample Temperature: 180 °C
       Reservoir, 75 eV
    

          27.0      11.5
          29.0      16.4
          39.0      13.4
          40.0       2.8
          41.0      31.2
          42.0      13.1
          43.0     100.0
          44.0       3.3
          51.0       1.2
          53.0       4.7
          54.0       1.4
          55.0      44.7
          56.0      31.0
          57.0      32.5
          58.0       1.4
          67.0       3.8
          68.0      10.8
          69.0      16.1
          70.0      72.0
          71.0      20.7
          72.0       1.0
          81.0       1.0
          83.0      19.1
          84.0       4.7
          85.0       1.0
          95.0       1.1
         109.0       1.2
         111.0       1.2
         126.0       7.9
    

400 MHz in CDCl3

90 MHz in CDCl3


  • 1H NMR 399.65 MHz
    C9 H18 0.05 ml : 0.5 ml CDCl3
    2,4-dimethyl-1-heptene
    ChemicalStructure
        Assign.     Shift(ppm)
    A *1 4.723 B *1 4.644 C *2 2.012 D *2 1.791 E 1.680 F 1.614 G *3 1.38 J 1.28 K *3 1.07 L 0.886 M 0.829 J(D,C)=13.5HZ. J(F,D)=8.3HZ. J(C,F)=6.2HZ.

         Hz     ppm     Int.
    

       1889.40   4.728    150
       1888.31   4.725    192
       1887.21   4.723    202
       1885.99   4.720    165
       1857.30   4.648    180
       1856.32   4.645    205
       1855.35   4.643    193
        814.82   2.039     77
        808.59   2.024     83
        801.27   2.005    100
        795.17   1.990    103
        726.56   1.818    108
        725.83   1.817    114
        718.26   1.798    130
        717.41   1.796    135
        713.13   1.785     80
        712.28   1.783     83
        704.83   1.764    103
        703.98   1.762    107
        671.39   1.680    880
        661.62   1.656     31
        659.91   1.652     41
        658.33   1.648     37
        657.10   1.645     31
        655.15   1.640     41
        653.44   1.636     53
        651.86   1.632     53
        650.39   1.628     35
        648.68   1.624     50
        646.97   1.619     66
        645.39   1.615     68
        643.68   1.611     43
        642.21   1.607     47
        640.50   1.603     69
        638.92   1.599     74
        637.70   1.596     51
        634.16   1.587     46
        632.45   1.583     44
        557.74   1.396     45
        555.30   1.390     49
        552.61   1.383     59
        550.42   1.378     66
        547.97   1.372     51
        545.53   1.366     77
        543.33   1.360     60
        541.02   1.354     39
        538.33   1.348     50
        536.01   1.342     70
        535.16   1.340     55
        529.05   1.324     54
        527.22   1.320     89
        525.15   1.315     46
        523.93   1.311     36
        521.97   1.307    161
        520.14   1.302     68
        518.31   1.297     42
        516.97   1.294     81
        514.89   1.289    138
        513.18   1.285    128
        510.99   1.279    102
        509.64   1.276    116
        508.30   1.272    117
        507.32   1.270     98
        505.37   1.265    104
        503.05   1.259     98
        500.49   1.253     38
        498.17   1.247     92
        496.34   1.242     59
        492.68   1.233     43
        491.82   1.231     41
        443.85   1.111     42
        442.75   1.108     41
        437.99   1.096     39
        435.42   1.090     82
        432.37   1.082     65
        431.27   1.080     51
        430.18   1.077     64
        427.49   1.070     84
        424.32   1.062     61
        422.24   1.057     60
        419.56   1.050     48
        367.68   0.921     32
        367.07   0.919     32
        363.53   0.910     78
        361.08   0.904    473
        354.13   0.887    795
        349.73   0.876    107
        348.63   0.873    113
        346.80   0.868    404
        342.53   0.858     54
        341.55   0.855     46
        334.47   0.837   1000
        327.88   0.821    936
    


  • 1H NMR 89.56 MHz
    C9 H18 0.05 ml : 0.5 ml CDCl3
    2,4-dimethyl-1-heptene
    ChemicalStructure
        Assign.     Shift(ppm)
    A *1 4.72 B *1 4.65 C *2 2.00 D *2 1.78 E 1.683 F 1.74 to 0.96 G 0.89 J 0.83

         Hz     ppm     Int.
    

        424.81   4.744     97
        423.50   4.729    145
        422.44   4.717    187
        421.13   4.703    164
        421.00   4.701    164
        419.56   4.685     75
        418.19   4.670    115
        417.25   4.659    187
        416.31   4.649    200
        413.81   4.621    104
        186.69   2.085     36
        186.38   2.082     38
        186.06   2.078     38
        179.31   2.003     91
        173.63   1.939     78
        169.94   1.898    129
        169.06   1.888    120
        162.56   1.816    183
        161.88   1.808    175
        151.44   1.691    742
        150.56   1.682   1000
        149.56   1.670    745
        143.69   1.605     56
        142.19   1.588     64
        141.50   1.580     59
        139.75   1.561     52
        139.38   1.557     51
        139.19   1.555     51
        138.44   1.546     55
        137.69   1.538     50
        137.13   1.532     51
        136.25   1.522     55
        133.88   1.495     46
        132.56   1.481     32
        132.19   1.476     32
        130.19   1.454     45
        128.50   1.435     58
        127.56   1.425     59
        126.13   1.409     60
        124.94   1.396     66
        123.38   1.378    123
        121.63   1.359    107
        120.50   1.346     84
        118.94   1.329     96
        118.56   1.324     96
        116.31   1.299    181
        115.25   1.287    129
        112.44   1.256    187
        110.31   1.232    187
        109.44   1.222    165
        108.13   1.208    161
        105.44   1.178    110
        103.50   1.156    111
        102.19   1.142     73
        100.13   1.119     52
         99.31   1.109     56
         97.69   1.091     58
         96.38   1.077     61
         96.13   1.074     61
         94.75   1.058     65
         93.88   1.049     55
         92.31   1.031     50
         90.06   1.006     57
         89.13   0.996     50
         85.50   0.955    276
         83.13   0.929    124
         81.63   0.912    169
         79.44   0.888    511
         77.31   0.864    810
         75.00   0.838    188
         74.63   0.834    189
         73.25   0.818    240
         71.19   0.795    671
    

in CDCl3



liquid film